Open Access
The Reactions of N,N′-Diphenyldithiomalondiamide with Arylmethylidene Meldrum’s Acids
Тип публикации: Journal Article
Дата публикации: 2022-12-15
scimago Q1
wos Q1
БС1
SJR: 1.273
CiteScore: 9.0
Impact factor: 4.9
ISSN: 16616596, 14220067
PubMed ID:
36555639
Catalysis
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Computer Science Applications
Spectroscopy
Molecular Biology
General Medicine
Краткое описание
The Michael addition reaction between dithiomalondianilide (N,N′-diphenyldithiomalondiamide) and arylmethylidene Meldrum’s acids, accompanied by subsequent heterocyclization, was investigated along with factors affecting the mixture composition of the obtained products. The plausible mechanism includes the formation of stable Michael adducts which, under the studied conditions, undergo further transformations to yield corresponding N-methylmorpholinium 4-aryl-6-oxo-3-(N-phenylthio-carbamoyl)-1,4,5,6-tetrahydropyridin-2- thiolates and their oxidation derivatives, 4,5-dihydro-3H-[1,2]dithiolo[3,4-b]pyridin-6(7H)-ones. The structure of one such product, N-methylmorpholinium 2,2-dimethyl-5-(1-(2-nitrophenyl)-3-(phenylamino)-2-(N-phenylthiocarbamoyl)-3-thioxopropyl)-4-oxo-4H-1,3-dioxin-6-olate, was confirmed via X-ray crystallography.
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Dotsenko V. V. et al. The Reactions of N,N′-Diphenyldithiomalondiamide with Arylmethylidene Meldrum’s Acids // International Journal of Molecular Sciences. 2022. Vol. 23. No. 24. p. 15997.
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Dotsenko V. V., Aksenov A., Sinotsko A. E., Varzieva E. A., Russkikh A. A., Levchenko A. G., Aksenov N. A., Aksenova I. V. The Reactions of N,N′-Diphenyldithiomalondiamide with Arylmethylidene Meldrum’s Acids // International Journal of Molecular Sciences. 2022. Vol. 23. No. 24. p. 15997.
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TY - JOUR
DO - 10.3390/ijms232415997
UR - https://doi.org/10.3390/ijms232415997
TI - The Reactions of N,N′-Diphenyldithiomalondiamide with Arylmethylidene Meldrum’s Acids
T2 - International Journal of Molecular Sciences
AU - Dotsenko, Viktor V
AU - Aksenov, Alexander V.
AU - Sinotsko, Anna E
AU - Varzieva, Ekaterina A
AU - Russkikh, Alena A
AU - Levchenko, Arina G
AU - Aksenov, Nicolai A
AU - Aksenova, Inna V
PY - 2022
DA - 2022/12/15
PB - MDPI
SP - 15997
IS - 24
VL - 23
PMID - 36555639
SN - 1661-6596
SN - 1422-0067
ER -
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@article{2022_Dotsenko,
author = {Viktor V Dotsenko and Alexander V. Aksenov and Anna E Sinotsko and Ekaterina A Varzieva and Alena A Russkikh and Arina G Levchenko and Nicolai A Aksenov and Inna V Aksenova},
title = {The Reactions of N,N′-Diphenyldithiomalondiamide with Arylmethylidene Meldrum’s Acids},
journal = {International Journal of Molecular Sciences},
year = {2022},
volume = {23},
publisher = {MDPI},
month = {dec},
url = {https://doi.org/10.3390/ijms232415997},
number = {24},
pages = {15997},
doi = {10.3390/ijms232415997}
}
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Dotsenko, Viktor V., et al. “The Reactions of N,N′-Diphenyldithiomalondiamide with Arylmethylidene Meldrum’s Acids.” International Journal of Molecular Sciences, vol. 23, no. 24, Dec. 2022, p. 15997. https://doi.org/10.3390/ijms232415997.
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