Open Access
Exploring the Conformational Equilibrium of Mefenamic Acid Released from Silica Aerogels via NMR Analysis
Тип публикации: Journal Article
Дата публикации: 2023-04-07
SCImago Q1
Tоп 10% SCImago
WOS Q1
БС1
SJR: 1.316
CiteScore: 10
Impact factor: 5.6
ISSN: 16616596, 14220067
PubMed ID:
37108046
Catalysis
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Computer Science Applications
Spectroscopy
Molecular Biology
General Medicine
Краткое описание
This study examines the influence of mefenamic acid on the physical and chemical properties of silica aerogels, as well as its effect on the sorption characteristics of the composite material. Solid state magic angle spinning nuclear magnetic resonance (MAS NMR) and high-pressure 13C NMR kinetic studies were conducted to identify the presence of mefenamic acid and measure the kinetic rates of CO2 sorption. Additionally, a high-pressure T1–T2 relaxation-relaxation correlation spectroscopy (RRCOSY) study was conducted to estimate the relative amount of mefenamic acid in the aerogel’s pores, and a high-pressure nuclear Overhauser effect spectoscopy (NOESY) study was conducted to investigate the conformational preference of mefenamic acid released from the aerogel. The results indicate that mefenamic acid is affected by the chemical environment of the aerogel, altering the ratio of mefenamic acid conformers from 75% to 25% in its absence to 22% to 78% in the presence of aerogel.
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(38.89%)
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ГОСТ
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Khodov I. A. et al. Exploring the Conformational Equilibrium of Mefenamic Acid Released from Silica Aerogels via NMR Analysis // International Journal of Molecular Sciences. 2023. Vol. 24. No. 8. p. 6882.
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Khodov I. A., Sobornova V. V., Mulloyarova V., Belov K. V., Dyshin A. A., Batista de Carvalho L. A. E., Tolstoy P. M., Kiselev M. Exploring the Conformational Equilibrium of Mefenamic Acid Released from Silica Aerogels via NMR Analysis // International Journal of Molecular Sciences. 2023. Vol. 24. No. 8. p. 6882.
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RIS
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TY - JOUR
DO - 10.3390/ijms24086882
UR - https://doi.org/10.3390/ijms24086882
TI - Exploring the Conformational Equilibrium of Mefenamic Acid Released from Silica Aerogels via NMR Analysis
T2 - International Journal of Molecular Sciences
AU - Khodov, Ilya A.
AU - Sobornova, Valentina V
AU - Mulloyarova, Valeriya
AU - Belov, Konstantin V.
AU - Dyshin, Alexey A.
AU - Batista de Carvalho, Luís A. E.
AU - Tolstoy, Peter M.
AU - Kiselev, Michael
PY - 2023
DA - 2023/04/07
PB - MDPI
SP - 6882
IS - 8
VL - 24
PMID - 37108046
SN - 1661-6596
SN - 1422-0067
ER -
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@article{2023_Khodov,
author = {Ilya A. Khodov and Valentina V Sobornova and Valeriya Mulloyarova and Konstantin V. Belov and Alexey A. Dyshin and Luís A. E. Batista de Carvalho and Peter M. Tolstoy and Michael Kiselev},
title = {Exploring the Conformational Equilibrium of Mefenamic Acid Released from Silica Aerogels via NMR Analysis},
journal = {International Journal of Molecular Sciences},
year = {2023},
volume = {24},
publisher = {MDPI},
month = {apr},
url = {https://doi.org/10.3390/ijms24086882},
number = {8},
pages = {6882},
doi = {10.3390/ijms24086882}
}
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MLA
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Khodov, Ilya A., et al. “Exploring the Conformational Equilibrium of Mefenamic Acid Released from Silica Aerogels via NMR Analysis.” International Journal of Molecular Sciences, vol. 24, no. 8, Apr. 2023, p. 6882. https://doi.org/10.3390/ijms24086882.
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