Open Access
One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes
Publication type: Journal Article
Publication date: 2019-10-06
PubMed ID:
31590462
Organic Chemistry
Drug Discovery
Physical and Theoretical Chemistry
Pharmaceutical Science
Molecular Medicine
Analytical Chemistry
Chemistry (miscellaneous)
Abstract
The reaction of pyridines with trifluoroacetylated acetylenes was investigated. It was found that the reaction of various pyridines with two molecules of CF3CO-acetylenes proceeds under mild metal-free conditions. As a result, efficient stereoselective synthesis of 3-arylethynyl-3-trifluoromethyl-1,3-oxazinopyridines was elaborated. Target heterocycles can be prepared in up to quantitative yields.
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Metrics
16
Total citations:
16
Citations from 2024:
6
(37.5%)
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GOST
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Muzalevskiy et al. One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes // Molecules. 2019. Vol. 24. No. 19. p. 3594.
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Muzalevskiy, Sizova, Belyaeva, Trofimov, Nenajdenko One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes // Molecules. 2019. Vol. 24. No. 19. p. 3594.
Cite this
RIS
Copy
TY - JOUR
DO - 10.3390/molecules24193594
UR - https://doi.org/10.3390/molecules24193594
TI - One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes
T2 - Molecules
AU - Muzalevskiy
AU - Sizova
AU - Belyaeva
AU - Trofimov
AU - Nenajdenko
PY - 2019
DA - 2019/10/06
PB - MDPI
SP - 3594
IS - 19
VL - 24
PMID - 31590462
SN - 1420-3049
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2019_Muzalevskiy,
author = {Muzalevskiy and Sizova and Belyaeva and Trofimov and Nenajdenko},
title = {One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes},
journal = {Molecules},
year = {2019},
volume = {24},
publisher = {MDPI},
month = {oct},
url = {https://doi.org/10.3390/molecules24193594},
number = {19},
pages = {3594},
doi = {10.3390/molecules24193594}
}
Cite this
MLA
Copy
Muzalevskiy, et al. “One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes.” Molecules, vol. 24, no. 19, Oct. 2019, p. 3594. https://doi.org/10.3390/molecules24193594.