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One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes
Тип публикации: Journal Article
Дата публикации: 2019-10-06
PubMed ID:
31590462
Organic Chemistry
Drug Discovery
Physical and Theoretical Chemistry
Pharmaceutical Science
Molecular Medicine
Analytical Chemistry
Chemistry (miscellaneous)
Краткое описание
The reaction of pyridines with trifluoroacetylated acetylenes was investigated. It was found that the reaction of various pyridines with two molecules of CF3CO-acetylenes proceeds under mild metal-free conditions. As a result, efficient stereoselective synthesis of 3-arylethynyl-3-trifluoromethyl-1,3-oxazinopyridines was elaborated. Target heterocycles can be prepared in up to quantitative yields.
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Muzalevskiy et al. One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes // Molecules. 2019. Vol. 24. No. 19. p. 3594.
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Muzalevskiy, Sizova, Belyaeva, Trofimov, Nenajdenko One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes // Molecules. 2019. Vol. 24. No. 19. p. 3594.
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TY - JOUR
DO - 10.3390/molecules24193594
UR - https://doi.org/10.3390/molecules24193594
TI - One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes
T2 - Molecules
AU - Muzalevskiy
AU - Sizova
AU - Belyaeva
AU - Trofimov
AU - Nenajdenko
PY - 2019
DA - 2019/10/06
PB - MDPI
SP - 3594
IS - 19
VL - 24
PMID - 31590462
SN - 1420-3049
ER -
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@article{2019_Muzalevskiy,
author = {Muzalevskiy and Sizova and Belyaeva and Trofimov and Nenajdenko},
title = {One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes},
journal = {Molecules},
year = {2019},
volume = {24},
publisher = {MDPI},
month = {oct},
url = {https://doi.org/10.3390/molecules24193594},
number = {19},
pages = {3594},
doi = {10.3390/molecules24193594}
}
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MLA
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Muzalevskiy, et al. “One-Pot Metal-Free Synthesis of 3-CF3-1,3-Oxazinopyridines by Reaction of Pyridines with CF3CO-Acetylenes.” Molecules, vol. 24, no. 19, Oct. 2019, p. 3594. https://doi.org/10.3390/molecules24193594.