Open Access
Microwave Synthesis of Copper Phyllosilicates as Effective Catalysts for Hydrogenation of C≡C Bonds
Anastasiya Shesterkina
1, 2
,
Kseniia Vikanova
2
,
Anna Strekalova
1, 2
,
Elena Shuvalova
2
,
Gennady Kapustin
2
,
Tapio Salmi
3
Тип публикации: Journal Article
Дата публикации: 2022-02-01
PubMed ID:
35164251
Organic Chemistry
Drug Discovery
Physical and Theoretical Chemistry
Pharmaceutical Science
Molecular Medicine
Analytical Chemistry
Chemistry (miscellaneous)
Краткое описание
For the first time, the new microwave-assisted method for the synthesis of copper phyllosilicates on a commercial SiO2 carrier was developed. The application of microwave synthesis allowed to decrease the synthesis time from 9 to 6 h compared to the traditional DPU method of preparing chrysocolla. The synthesized catalysts were studied by N2 adsorption, TEM and XRD methods. Catalysts prepared by microwave method are highly effective in the selective hydrogenation of the С≡С bond in 1,4-butynediol to 1,4-butenediol and 2-phenylethinylaniline with a selectivity of 96.5% and 100% at full conversion for 2 and 0.5 h of the reaction, respectively.
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Shesterkina A. et al. Microwave Synthesis of Copper Phyllosilicates as Effective Catalysts for Hydrogenation of C≡C Bonds // Molecules. 2022. Vol. 27. No. 3. p. 988.
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Shesterkina A., Vikanova K., Kostyukhin E. M., Strekalova A., Shuvalova E., Kapustin G., Salmi T. Microwave Synthesis of Copper Phyllosilicates as Effective Catalysts for Hydrogenation of C≡C Bonds // Molecules. 2022. Vol. 27. No. 3. p. 988.
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TY - JOUR
DO - 10.3390/molecules27030988
UR - https://doi.org/10.3390/molecules27030988
TI - Microwave Synthesis of Copper Phyllosilicates as Effective Catalysts for Hydrogenation of C≡C Bonds
T2 - Molecules
AU - Shesterkina, Anastasiya
AU - Vikanova, Kseniia
AU - Kostyukhin, Egor M
AU - Strekalova, Anna
AU - Shuvalova, Elena
AU - Kapustin, Gennady
AU - Salmi, Tapio
PY - 2022
DA - 2022/02/01
PB - MDPI
SP - 988
IS - 3
VL - 27
PMID - 35164251
SN - 1420-3049
ER -
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@article{2022_Shesterkina,
author = {Anastasiya Shesterkina and Kseniia Vikanova and Egor M Kostyukhin and Anna Strekalova and Elena Shuvalova and Gennady Kapustin and Tapio Salmi},
title = {Microwave Synthesis of Copper Phyllosilicates as Effective Catalysts for Hydrogenation of C≡C Bonds},
journal = {Molecules},
year = {2022},
volume = {27},
publisher = {MDPI},
month = {feb},
url = {https://doi.org/10.3390/molecules27030988},
number = {3},
pages = {988},
doi = {10.3390/molecules27030988}
}
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MLA
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Shesterkina, Anastasiya, et al. “Microwave Synthesis of Copper Phyllosilicates as Effective Catalysts for Hydrogenation of C≡C Bonds.” Molecules, vol. 27, no. 3, Feb. 2022, p. 988. https://doi.org/10.3390/molecules27030988.