Open Access
Imine Palladacycles: Synthesis, Structural Analysis and Application in Suzuki–Miyaura Cross Coupling in Semi-Aqueous Media
Publication type: Journal Article
Publication date: 2022-05-14
PubMed ID:
35630622
Organic Chemistry
Drug Discovery
Physical and Theoretical Chemistry
Pharmaceutical Science
Molecular Medicine
Analytical Chemistry
Chemistry (miscellaneous)
Abstract
Treatment of the imines a–c with palladium(II) acetate in acetic acid yielded the μ-acetate dinuclear complexes 1a–c, which readily reacted with sodium chloride or bromide to provide μ-halide analogues. The reaction of the latter with nitrogen, phosphorus and oxygen donor nucleophiles yielded new imine palladacycles following the cleavage of the Pd2X2 unit. The complexes were fully characterized by microanalysis, 1H, 13C and 31P NMR spectroscopies, as appropriate. The compounds were applied as catalysts in the Suzuki–Miyaura coupling reaction in aqueous and semi-aqueous media.
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Bermúdez Puente B. et al. Imine Palladacycles: Synthesis, Structural Analysis and Application in Suzuki–Miyaura Cross Coupling in Semi-Aqueous Media // Molecules. 2022. Vol. 27. No. 10. p. 3146.
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Bermúdez Puente B., Adrio L. A., Lucio Martínez F., Reigosa F., Ortigueira J. M., Vila J. M. Imine Palladacycles: Synthesis, Structural Analysis and Application in Suzuki–Miyaura Cross Coupling in Semi-Aqueous Media // Molecules. 2022. Vol. 27. No. 10. p. 3146.
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RIS
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TY - JOUR
DO - 10.3390/molecules27103146
UR - https://doi.org/10.3390/molecules27103146
TI - Imine Palladacycles: Synthesis, Structural Analysis and Application in Suzuki–Miyaura Cross Coupling in Semi-Aqueous Media
T2 - Molecules
AU - Bermúdez Puente, Brais
AU - Adrio, Luis A
AU - Lucio Martínez, Fátima
AU - Reigosa, Francisco
AU - Ortigueira, J. M.
AU - Vila, José M
PY - 2022
DA - 2022/05/14
PB - MDPI
SP - 3146
IS - 10
VL - 27
PMID - 35630622
SN - 1420-3049
ER -
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BibTex (up to 50 authors)
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@article{2022_Bermúdez Puente,
author = {Brais Bermúdez Puente and Luis A Adrio and Fátima Lucio Martínez and Francisco Reigosa and J. M. Ortigueira and José M Vila},
title = {Imine Palladacycles: Synthesis, Structural Analysis and Application in Suzuki–Miyaura Cross Coupling in Semi-Aqueous Media},
journal = {Molecules},
year = {2022},
volume = {27},
publisher = {MDPI},
month = {may},
url = {https://doi.org/10.3390/molecules27103146},
number = {10},
pages = {3146},
doi = {10.3390/molecules27103146}
}
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MLA
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Bermúdez Puente, Brais, et al. “Imine Palladacycles: Synthesis, Structural Analysis and Application in Suzuki–Miyaura Cross Coupling in Semi-Aqueous Media.” Molecules, vol. 27, no. 10, May. 2022, p. 3146. https://doi.org/10.3390/molecules27103146.