Open Access
A Two-Step Synthesis of Unprotected 3-Aminoindoles via Post Functionalization with Nitrostyrene
Тип публикации: Journal Article
Дата публикации: 2023-04-23
PubMed ID:
37175067
Organic Chemistry
Drug Discovery
Physical and Theoretical Chemistry
Pharmaceutical Science
Molecular Medicine
Analytical Chemistry
Chemistry (miscellaneous)
Краткое описание
A novel, low-cost method for the preparation of not easily accessible free 3-aminoindoles has been developed. This approach is based on a well-established reaction between indoles and nitrostyrene in the presence of phosphorous acid, which results in the formation of 4′-phenyl-4′H-spiro[indole-3,5′-isoxazoles]. The latter could be transformed to corresponding aminated indoles by reaction with hydrazine hydrate in good or excellent yields upon microwave-assisted heating.
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ГОСТ
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Aksenov N. A. et al. A Two-Step Synthesis of Unprotected 3-Aminoindoles via Post Functionalization with Nitrostyrene // Molecules. 2023. Vol. 28. No. 9. p. 3657.
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Aksenov N. A., Arutiunov N. A., Kurenkov I. A., Malyuga V. V., Aksenov D. A., Momotova D. S., Zatsepilina A. M., Chukanova E. A., Leontiev A. V., Aksenov A. A Two-Step Synthesis of Unprotected 3-Aminoindoles via Post Functionalization with Nitrostyrene // Molecules. 2023. Vol. 28. No. 9. p. 3657.
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TY - JOUR
DO - 10.3390/molecules28093657
UR - https://doi.org/10.3390/molecules28093657
TI - A Two-Step Synthesis of Unprotected 3-Aminoindoles via Post Functionalization with Nitrostyrene
T2 - Molecules
AU - Aksenov, Nicolai A.
AU - Arutiunov, Nikolai A
AU - Kurenkov, Igor A
AU - Malyuga, Vladimir V
AU - Aksenov, Dmitrii A
AU - Momotova, Daria S
AU - Zatsepilina, Anna M.
AU - Chukanova, Elizaveta A.
AU - Leontiev, Alexander V.
AU - Aksenov, Alexander V.
PY - 2023
DA - 2023/04/23
PB - MDPI
SP - 3657
IS - 9
VL - 28
PMID - 37175067
SN - 1420-3049
ER -
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BibTex (до 50 авторов)
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@article{2023_Aksenov,
author = {Nicolai A. Aksenov and Nikolai A Arutiunov and Igor A Kurenkov and Vladimir V Malyuga and Dmitrii A Aksenov and Daria S Momotova and Anna M. Zatsepilina and Elizaveta A. Chukanova and Alexander V. Leontiev and Alexander V. Aksenov},
title = {A Two-Step Synthesis of Unprotected 3-Aminoindoles via Post Functionalization with Nitrostyrene},
journal = {Molecules},
year = {2023},
volume = {28},
publisher = {MDPI},
month = {apr},
url = {https://doi.org/10.3390/molecules28093657},
number = {9},
pages = {3657},
doi = {10.3390/molecules28093657}
}
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MLA
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Aksenov, Nicolai A., et al. “A Two-Step Synthesis of Unprotected 3-Aminoindoles via Post Functionalization with Nitrostyrene.” Molecules, vol. 28, no. 9, Apr. 2023, p. 3657. https://doi.org/10.3390/molecules28093657.
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