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Open access
MDPI
Nanomaterials
,  volume 11 ,  issue 9 ,  pages 2388

X-ray Fluorescence Spectroscopy Features of Micro- and Nanoscale Copper and Nickel Particle Compositions

Publication type: Journal Article
Publication date: 2021-09-14
MDPI
scimago Q1
wos Q2
SJR: 0.811
CiteScore: 9.2
Impact factor: 4.3
ISSN: 20794991
DOI:  10.3390/nano11092388
PubMed ID:  34578704
General Chemical Engineering
General Materials Science
Abstract

The study is devoted to X-ray fluorescence spectroscopy (XRF) features of micro- and nanosized powder mixtures of copper and nickel. XRF is a high accuracy method that allows for both qualitative and quantitative analysis. However, the XRF measurement error due to the size of the studied particles is not usually taken into account, which limits the use of the method in some cases, such as analysis of Ni-Cu mixtures and coatings. In this paper, a method for obtaining copper and nickel nanoparticles was investigated, and the XRF of powder compositions was considered in detail. The initial micro- and nanoparticles of copper and nickel were studied in detail using SEM, TEM, XRD, and EDX. Based on experimental data, calibration curves for copper-nickel powder compositions of various sizes were developed. According to the results, it was experimentally established that the calibration curves constructed for nanoscale and microscale powders differ significantly. The presented approach can be expanded for other metals and particle sizes.

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GOST |
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GOST Copy
Chebakova K. A. et al. X-ray Fluorescence Spectroscopy Features of Micro- and Nanoscale Copper and Nickel Particle Compositions // Nanomaterials. 2021. Vol. 11. No. 9. p. 2388.
GOST all authors (up to 50) Copy
Chebakova K. A., Dzidziguri E. L., Sidorova E. N., Vasiliev A. A., Ozherelkov D. Y., Pelevin I., Gromov A. A., Nalivaiko A. Y. X-ray Fluorescence Spectroscopy Features of Micro- and Nanoscale Copper and Nickel Particle Compositions // Nanomaterials. 2021. Vol. 11. No. 9. p. 2388.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.3390/nano11092388
UR - https://doi.org/10.3390/nano11092388
TI - X-ray Fluorescence Spectroscopy Features of Micro- and Nanoscale Copper and Nickel Particle Compositions
T2 - Nanomaterials
AU - Chebakova, Kristina A
AU - Dzidziguri, Ella L.
AU - Sidorova, Elena N
AU - Vasiliev, Andrey A
AU - Ozherelkov, Dmitriy Yu.
AU - Pelevin, Ivan
AU - Gromov, Alexander A
AU - Nalivaiko, Anton Yu.
PY - 2021
DA - 2021/09/14
PB - MDPI
SP - 2388
IS - 9
VL - 11
PMID - 34578704
SN - 2079-4991
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2021_Chebakova,
author = {Kristina A Chebakova and Ella L. Dzidziguri and Elena N Sidorova and Andrey A Vasiliev and Dmitriy Yu. Ozherelkov and Ivan Pelevin and Alexander A Gromov and Anton Yu. Nalivaiko},
title = {X-ray Fluorescence Spectroscopy Features of Micro- and Nanoscale Copper and Nickel Particle Compositions},
journal = {Nanomaterials},
year = {2021},
volume = {11},
publisher = {MDPI},
month = {sep},
url = {https://doi.org/10.3390/nano11092388},
number = {9},
pages = {2388},
doi = {10.3390/nano11092388}
}
MLA
Cite this
MLA Copy
Chebakova, Kristina A., et al. “X-ray Fluorescence Spectroscopy Features of Micro- and Nanoscale Copper and Nickel Particle Compositions.” Nanomaterials, vol. 11, no. 9, Sep. 2021, p. 2388. https://doi.org/10.3390/nano11092388.