Study on Synthesis of (R)-tert-butyl (1-hydroxybut-3-yn-2-yl)carbamate
Publication type: Journal Article
Publication date: 2014-01-16
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ISSN: 16628985, 10226680
General Engineering
Abstract
(R)-tert-butyl (1-hydroxybut-3-yn-2-yl) carbamate, an key intermediate of the natural product jaspine B which was isolated from various sponges and endowed with cytotoxic activity against several human carcinoma cell lines, was synthesized fromL-Serine in overall yield 41% through seven steps, including esterification, Boc protection, acetonization, reduction,Corey-Fuchs reaction and deprotection.
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Tang L. J. et al. Study on Synthesis of (R)-tert-butyl (1-hydroxybut-3-yn-2-yl)carbamate // Advanced Materials Research. 2014. Vol. 881-883. pp. 438-441.
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Tang L. J., Lv C. S., Liu D. W., Qin S. L., Wang L. P., Li Yu. P., Wang X. J., Huang S. P. Study on Synthesis of (R)-tert-butyl (1-hydroxybut-3-yn-2-yl)carbamate // Advanced Materials Research. 2014. Vol. 881-883. pp. 438-441.
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TY - JOUR
DO - 10.4028/www.scientific.net/amr.881-883.438
UR - https://doi.org/10.4028/www.scientific.net/amr.881-883.438
TI - Study on Synthesis of (R)-tert-butyl (1-hydroxybut-3-yn-2-yl)carbamate
T2 - Advanced Materials Research
AU - Tang, Lin Jun
AU - Lv, Chang Shan
AU - Liu, Dong Wang
AU - Qin, Shuang Lin
AU - Wang, Li Ping
AU - Li, Yu Ping
AU - Wang, Xiao Ji
AU - Huang, Shuang Ping
PY - 2014
DA - 2014/01/16
PB - Trans Tech Publications
SP - 438-441
VL - 881-883
SN - 1662-8985
SN - 1022-6680
ER -
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@article{2014_Tang,
author = {Lin Jun Tang and Chang Shan Lv and Dong Wang Liu and Shuang Lin Qin and Li Ping Wang and Yu Ping Li and Xiao Ji Wang and Shuang Ping Huang},
title = {Study on Synthesis of (R)-tert-butyl (1-hydroxybut-3-yn-2-yl)carbamate},
journal = {Advanced Materials Research},
year = {2014},
volume = {881-883},
publisher = {Trans Tech Publications},
month = {jan},
url = {https://doi.org/10.4028/www.scientific.net/amr.881-883.438},
pages = {438--441},
doi = {10.4028/www.scientific.net/amr.881-883.438}
}