Structurally Diverse Bench‐Stable Nickel(0) Pre‐Catalysts: A Practical Toolkit for In Situ Ligation Protocols
T Tran-Van
1
,
Nana Kim
1
,
Camille Z Rubel
1
,
Xiangyu Wu
2
,
Taeho Kang
1
,
Tanner C Jankins
1
,
Zi-Qi Li
1
,
Sloan Ayers
3
,
Milan Gembicky
4
,
Jake B Bailey
4
,
Emily J Sturgell
1
,
Brittany B Sanchez
1
,
Jason Chen
1
,
Song Lin
2
,
Тип публикации: Journal Article
Дата публикации: 2023-01-18
scimago Q1
wos Q1
БС1
SJR: 5.550
CiteScore: 27.6
Impact factor: 16.9
ISSN: 14337851, 15213773
PubMed ID:
36524997
General Chemistry
Catalysis
Краткое описание
A flurry of recent research has centered on harnessing the power of nickel catalysis in organic synthesis. These efforts have been bolstered by contemporaneous development of well-defined nickel (pre)catalysts with diverse structure and reactivity. In this report, we present ten different bench-stable, 18-electron, formally zero-valent nickel-olefin complexes that are competent pre-catalysts in various reactions. Our investigation includes preparations of novel, bench stable Ni(COD)(L) complexes (COD = 1,5-cyclooctadiene), in which L = quinone, cyclopentadienone, thiophene-S-oxide, and fulvene. Characterization by NMR, IR, single-crystal X-ray diffraction, cyclic voltammetry, thermogravimetric analysis, and natural bond orbital analysis sheds light on the structure, bonding, and properties of these complexes. Applications in an assortment of nickel-catalyzed reactions underscore the complementary nature of the different pre-catalysts within this toolkit.
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Tran-Van T. et al. Structurally Diverse Bench‐Stable Nickel(0) Pre‐Catalysts: A Practical Toolkit for In Situ Ligation Protocols // Angewandte Chemie - International Edition. 2023. Vol. 62. No. 9.
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Tran-Van T., Kim N., Rubel C. Z., Wu X., Kang T., Jankins T. C., Li Z., Joannou M. V., Ayers S., Gembicky M., Bailey J. B., Sturgell E. J., Sanchez B. B., Chen J., Lin S., Eastgate M. D., Wisniewski S., Engle K. M. Structurally Diverse Bench‐Stable Nickel(0) Pre‐Catalysts: A Practical Toolkit for In Situ Ligation Protocols // Angewandte Chemie - International Edition. 2023. Vol. 62. No. 9.
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TY - JOUR
DO - 10.1002/anie.202211794
UR - https://doi.org/10.1002/anie.202211794
TI - Structurally Diverse Bench‐Stable Nickel(0) Pre‐Catalysts: A Practical Toolkit for In Situ Ligation Protocols
T2 - Angewandte Chemie - International Edition
AU - Tran-Van, T
AU - Kim, Nana
AU - Rubel, Camille Z
AU - Wu, Xiangyu
AU - Kang, Taeho
AU - Jankins, Tanner C
AU - Li, Zi-Qi
AU - Joannou, Matthew V
AU - Ayers, Sloan
AU - Gembicky, Milan
AU - Bailey, Jake B
AU - Sturgell, Emily J
AU - Sanchez, Brittany B
AU - Chen, Jason
AU - Lin, Song
AU - Eastgate, Martin D
AU - Wisniewski, Steven
AU - Engle, Keary M
PY - 2023
DA - 2023/01/18
PB - Wiley
IS - 9
VL - 62
PMID - 36524997
SN - 1433-7851
SN - 1521-3773
ER -
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BibTex (до 50 авторов)
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@article{2023_Tran-Van,
author = {T Tran-Van and Nana Kim and Camille Z Rubel and Xiangyu Wu and Taeho Kang and Tanner C Jankins and Zi-Qi Li and Matthew V Joannou and Sloan Ayers and Milan Gembicky and Jake B Bailey and Emily J Sturgell and Brittany B Sanchez and Jason Chen and Song Lin and Martin D Eastgate and Steven Wisniewski and Keary M Engle},
title = {Structurally Diverse Bench‐Stable Nickel(0) Pre‐Catalysts: A Practical Toolkit for In Situ Ligation Protocols},
journal = {Angewandte Chemie - International Edition},
year = {2023},
volume = {62},
publisher = {Wiley},
month = {jan},
url = {https://doi.org/10.1002/anie.202211794},
number = {9},
doi = {10.1002/anie.202211794}
}