volume 71 issue 6 pages 636-640

Determination of Ethinyl Estradiol in Solid Dosage Forms by High-Performance Liquid Chromatography

Suzanne H Strusiak 1
JOHN G. HOOGERHEIDE 1
Maureen S Gardner 1
1
 
Schering Corporation Bloomfield, NJ 07003.
Publication typeJournal Article
Publication date1982-06-01
scimago Q1
wos Q2
SJR0.737
CiteScore7.2
Impact factor3.8
ISSN00223549, 15206017
Pharmaceutical Science
Abstract
A rapid, reproducible high-performance liquid chromatographic system for the determination of ethinyl estradiol in solid dosage forms consisting of a reversed-phase column with a mobile phase of 0.05 M aqueous KH2PO4-methyl alcohol (2:3) and fluorescence detection has been developed. This stability-indicating method is applicable to tablets containing ethinyl estradiol alone or in combination with methyltestosterone and progesterones. The procedure has been used for the determination of ethinyl estradiol in single tablets, stability samples, and dissolution medium. Recovery of drug substance added to placebo was from 97.3 to 101.5% in stability and single-tablet assays, and 95.4 to 102.2% in dissolution assays. Reproducibility studies gave relative standard deviations of 0.4-2.2%.
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GOST Copy
Strusiak S. H., HOOGERHEIDE J. G., Gardner M. S. Determination of Ethinyl Estradiol in Solid Dosage Forms by High-Performance Liquid Chromatography // Journal of Pharmaceutical Sciences. 1982. Vol. 71. No. 6. pp. 636-640.
GOST all authors (up to 50) Copy
Strusiak S. H., HOOGERHEIDE J. G., Gardner M. S. Determination of Ethinyl Estradiol in Solid Dosage Forms by High-Performance Liquid Chromatography // Journal of Pharmaceutical Sciences. 1982. Vol. 71. No. 6. pp. 636-640.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1002/jps.2600710610
UR - https://doi.org/10.1002/jps.2600710610
TI - Determination of Ethinyl Estradiol in Solid Dosage Forms by High-Performance Liquid Chromatography
T2 - Journal of Pharmaceutical Sciences
AU - Strusiak, Suzanne H
AU - HOOGERHEIDE, JOHN G.
AU - Gardner, Maureen S
PY - 1982
DA - 1982/06/01
PB - Elsevier
SP - 636-640
IS - 6
VL - 71
PMID - 7097525
SN - 0022-3549
SN - 1520-6017
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{1982_Strusiak,
author = {Suzanne H Strusiak and JOHN G. HOOGERHEIDE and Maureen S Gardner},
title = {Determination of Ethinyl Estradiol in Solid Dosage Forms by High-Performance Liquid Chromatography},
journal = {Journal of Pharmaceutical Sciences},
year = {1982},
volume = {71},
publisher = {Elsevier},
month = {jun},
url = {https://doi.org/10.1002/jps.2600710610},
number = {6},
pages = {636--640},
doi = {10.1002/jps.2600710610}
}
MLA
Cite this
MLA Copy
Strusiak, Suzanne H., et al. “Determination of Ethinyl Estradiol in Solid Dosage Forms by High-Performance Liquid Chromatography.” Journal of Pharmaceutical Sciences, vol. 71, no. 6, Jun. 1982, pp. 636-640. https://doi.org/10.1002/jps.2600710610.