Polyazide Chemistry: The First Binary Group 6 Azides, Mo(N3)6, W(N3)6, [Mo(N3)7]?, and [W(N3)7]?, and the [NW(N3)4]? and [NMo(N3)4]? Ions
Ralf Haiges
1
,
Jerry A Boatz
2
,
Robert Bau
1
,
Stefan Schneider
1
,
Thorsten Schroer
1
,
Muhammed Yousufuddin
1
,
Karl O. Christe
1
2
Space and Missile Propulsion Division, Air Force Research Laboratory (AFRL/PRSP), 10 East Saturn Boulevard, Edwards Air Force Base, CA 93524, USA
|
Publication type: Journal Article
Publication date: 2005-03-11
scimago Q1
wos Q1
SJR: 5.550
CiteScore: 27.6
Impact factor: 16.9
ISSN: 14337851, 15213773
PubMed ID:
15723363
General Chemistry
Catalysis
Abstract
Bang on target: The highly explosive Group 6 azides Mo(N3)6 and W(N3)6 are prepared by the reaction of Me3SiN3 with MoF6 and WF6, respectively. The structure of W(N3)6 has perfect rhombohedral C3 symmetry (see picture). The reaction of Mo(N3)6 and W(N3)6 with ionic azides leads to the formation of [Mo(N3)7]− and [W(N3)7]−, respectively, the first binary heptaazides. Controlled decomposition of these anions produces [NMo(N3)4]− and [NW(N3)4]−.
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Haiges R. et al. Polyazide Chemistry: The First Binary Group 6 Azides, Mo(N3)6, W(N3)6, [Mo(N3)7]?, and [W(N3)7]?, and the [NW(N3)4]? and [NMo(N3)4]? Ions // Angewandte Chemie - International Edition. 2005. Vol. 44. No. 12. pp. 1860-1865.
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Haiges R., Boatz J. A., Bau R., Schneider S., Schroer T., Yousufuddin M., Christe K. O. Polyazide Chemistry: The First Binary Group 6 Azides, Mo(N3)6, W(N3)6, [Mo(N3)7]?, and [W(N3)7]?, and the [NW(N3)4]? and [NMo(N3)4]? Ions // Angewandte Chemie - International Edition. 2005. Vol. 44. No. 12. pp. 1860-1865.
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RIS
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TY - JOUR
DO - 10.1002/anie.200462740
UR - https://doi.org/10.1002/anie.200462740
TI - Polyazide Chemistry: The First Binary Group 6 Azides, Mo(N3)6, W(N3)6, [Mo(N3)7]?, and [W(N3)7]?, and the [NW(N3)4]? and [NMo(N3)4]? Ions
T2 - Angewandte Chemie - International Edition
AU - Haiges, Ralf
AU - Boatz, Jerry A
AU - Bau, Robert
AU - Schneider, Stefan
AU - Schroer, Thorsten
AU - Yousufuddin, Muhammed
AU - Christe, Karl O.
PY - 2005
DA - 2005/03/11
PB - Wiley
SP - 1860-1865
IS - 12
VL - 44
PMID - 15723363
SN - 1433-7851
SN - 1521-3773
ER -
Cite this
BibTex (up to 50 authors)
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@article{2005_Haiges,
author = {Ralf Haiges and Jerry A Boatz and Robert Bau and Stefan Schneider and Thorsten Schroer and Muhammed Yousufuddin and Karl O. Christe},
title = {Polyazide Chemistry: The First Binary Group 6 Azides, Mo(N3)6, W(N3)6, [Mo(N3)7]?, and [W(N3)7]?, and the [NW(N3)4]? and [NMo(N3)4]? Ions},
journal = {Angewandte Chemie - International Edition},
year = {2005},
volume = {44},
publisher = {Wiley},
month = {mar},
url = {https://doi.org/10.1002/anie.200462740},
number = {12},
pages = {1860--1865},
doi = {10.1002/anie.200462740}
}
Cite this
MLA
Copy
Haiges, Ralf, et al. “Polyazide Chemistry: The First Binary Group 6 Azides, Mo(N3)6, W(N3)6, [Mo(N3)7]?, and [W(N3)7]?, and the [NW(N3)4]? and [NMo(N3)4]? Ions.” Angewandte Chemie - International Edition, vol. 44, no. 12, Mar. 2005, pp. 1860-1865. https://doi.org/10.1002/anie.200462740.