2D NMR Trace Analysis by Continuous Hyperpolarization at High Magnetic Field
Publication type: Journal Article
Publication date: 2015-10-06
scimago Q1
wos Q1
SJR: 5.550
CiteScore: 27.6
Impact factor: 16.9
ISSN: 14337851, 15213773
PubMed ID:
26437608
General Chemistry
Catalysis
Abstract
Nuclear magnetic resonance is often the technique of choice in chemical analysis because of its sensitivity to molecular structure, quantitative character, and straightforward sample preparation. However, determination of trace analytes in complex mixtures is generally limited by low sensitivity and extensive signal overlap. Here, we present an approach for continuous hyperpolarization at high magnetic field that is based on signal amplification by reversible exchange (SABRE) and can be straightforwardly incorporated in multidimensional NMR experiments. This method was implemented in a 2D correlation experiment that allows detection and quantification of analytes at nanomolar concentration in complex solutions.
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93
Total citations:
93
Citations from 2025:
5
(5.38%)
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GOST
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Eshuis N. et al. 2D NMR Trace Analysis by Continuous Hyperpolarization at High Magnetic Field // Angewandte Chemie - International Edition. 2015. Vol. 54. No. 48. pp. 14527-14530.
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Eshuis N., Aspers R. L. E. G., Van Weerdenburg B. J. A., Feiters M., Rutjes F. P. J. T., Wijmenga S. S., Tessari M. 2D NMR Trace Analysis by Continuous Hyperpolarization at High Magnetic Field // Angewandte Chemie - International Edition. 2015. Vol. 54. No. 48. pp. 14527-14530.
Cite this
RIS
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TY - JOUR
DO - 10.1002/anie.201507831
UR - https://doi.org/10.1002/anie.201507831
TI - 2D NMR Trace Analysis by Continuous Hyperpolarization at High Magnetic Field
T2 - Angewandte Chemie - International Edition
AU - Eshuis, Nan
AU - Aspers, Ruud L. E. G.
AU - Van Weerdenburg, Bram J A
AU - Feiters, Martin
AU - Rutjes, Floris P. J. T.
AU - Wijmenga, Sybren S.
AU - Tessari, M.
PY - 2015
DA - 2015/10/06
PB - Wiley
SP - 14527-14530
IS - 48
VL - 54
PMID - 26437608
SN - 1433-7851
SN - 1521-3773
ER -
Cite this
BibTex (up to 50 authors)
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@article{2015_Eshuis,
author = {Nan Eshuis and Ruud L. E. G. Aspers and Bram J A Van Weerdenburg and Martin Feiters and Floris P. J. T. Rutjes and Sybren S. Wijmenga and M. Tessari},
title = {2D NMR Trace Analysis by Continuous Hyperpolarization at High Magnetic Field},
journal = {Angewandte Chemie - International Edition},
year = {2015},
volume = {54},
publisher = {Wiley},
month = {oct},
url = {https://doi.org/10.1002/anie.201507831},
number = {48},
pages = {14527--14530},
doi = {10.1002/anie.201507831}
}
Cite this
MLA
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Eshuis, Nan, et al. “2D NMR Trace Analysis by Continuous Hyperpolarization at High Magnetic Field.” Angewandte Chemie - International Edition, vol. 54, no. 48, Oct. 2015, pp. 14527-14530. https://doi.org/10.1002/anie.201507831.