Catalytic Oxo/Imido Heterometathesis by a Well-Defined Silica-Supported Titanium Imido Complex
Pavel A Zhizhko
1
,
Andrey V Pichugov
1, 2
,
Nikolai S Bushkov
1, 3
,
Florian Allouche
4
,
Anton A Zhizhin
1
,
Dmitry N. Zarubin
1
,
N. A. Ustynyuk
1
Publication type: Journal Article
Publication date: 2018-07-20
scimago Q1
wos Q1
SJR: 5.550
CiteScore: 27.6
Impact factor: 16.9
ISSN: 14337851, 15213773
PubMed ID:
29902359
General Chemistry
Catalysis
Abstract
Grafting Ti(=NtBu)(Me2 Pyr)2 (py)2 (Me2 Pyr= 2,5-dimethylpyrrolyl, py=pyridine) onto the surface of silica partially dehydroxylated at 700 °C gives the well-defined silica-supported Ti imido complex (≡SiO)Ti(=NtBu)(Me2 Pyr)(py)2 , which is fully characterized by IR and solid-state NMR spectroscopy as well as elemental and mass balance analyses. While stoichiometric imido-transfer reactivity is typical for Ti imides, the obtained surface complex is unique in that it enables catalytic transformations involving Ti imido and oxo intermediates. In particular, it efficiently catalyzes imidation of carbonyl compounds with N-sulfinylamines by oxo/imido heterometathesis.
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GOST
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Zhizhko P. A. et al. Catalytic Oxo/Imido Heterometathesis by a Well-Defined Silica-Supported Titanium Imido Complex // Angewandte Chemie - International Edition. 2018. Vol. 57. No. 34. pp. 10879-10882.
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Zhizhko P. A., Pichugov A. V., Bushkov N. S., Allouche F., Zhizhin A. A., Zarubin D. N., Ustynyuk N. A. Catalytic Oxo/Imido Heterometathesis by a Well-Defined Silica-Supported Titanium Imido Complex // Angewandte Chemie - International Edition. 2018. Vol. 57. No. 34. pp. 10879-10882.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1002/anie.201804346
UR - https://doi.org/10.1002/anie.201804346
TI - Catalytic Oxo/Imido Heterometathesis by a Well-Defined Silica-Supported Titanium Imido Complex
T2 - Angewandte Chemie - International Edition
AU - Zhizhko, Pavel A
AU - Pichugov, Andrey V
AU - Bushkov, Nikolai S
AU - Allouche, Florian
AU - Zhizhin, Anton A
AU - Zarubin, Dmitry N.
AU - Ustynyuk, N. A.
PY - 2018
DA - 2018/07/20
PB - Wiley
SP - 10879-10882
IS - 34
VL - 57
PMID - 29902359
SN - 1433-7851
SN - 1521-3773
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2018_Zhizhko,
author = {Pavel A Zhizhko and Andrey V Pichugov and Nikolai S Bushkov and Florian Allouche and Anton A Zhizhin and Dmitry N. Zarubin and N. A. Ustynyuk},
title = {Catalytic Oxo/Imido Heterometathesis by a Well-Defined Silica-Supported Titanium Imido Complex},
journal = {Angewandte Chemie - International Edition},
year = {2018},
volume = {57},
publisher = {Wiley},
month = {jul},
url = {https://doi.org/10.1002/anie.201804346},
number = {34},
pages = {10879--10882},
doi = {10.1002/anie.201804346}
}
Cite this
MLA
Copy
Zhizhko, Pavel A., et al. “Catalytic Oxo/Imido Heterometathesis by a Well-Defined Silica-Supported Titanium Imido Complex.” Angewandte Chemie - International Edition, vol. 57, no. 34, Jul. 2018, pp. 10879-10882. https://doi.org/10.1002/anie.201804346.