Chemical Recycling of Poly(Cyclohexene Carbonate) Using a Di‐Mg II Catalyst

Publication typeJournal Article
Publication date2022-05-05
scimago Q1
wos Q1
SJR5.550
CiteScore27.6
Impact factor16.9
ISSN14337851, 15213773
General Chemistry
Catalysis
Abstract
Chemical recycling of polymers to true monomers is pivotal for a circular plastics economy. Here, the first catalyzed chemical recycling of the widely investigated carbon dioxide derived polymer, poly(cyclohexene carbonate), to cyclohexene oxide and carbon dioxide is reported. The reaction requires dinuclear catalysis, with the di-MgII catalyst showing both high monomer selectivity (>98 %) and activity (TOF=150 h-1 , 0.33 mol %, 120 °C). The depolymerization occurs via a chain-end catalyzed depolymerization mechanism and DFT calculations indicate the high selectivity arises from Mg-alkoxide catalyzed epoxide extrusion being kinetically favorable compared to cyclic carbonate formation.
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GOST Copy
Singer F. N. et al. Chemical Recycling of Poly(Cyclohexene Carbonate) Using a Di‐Mg II Catalyst // Angewandte Chemie - International Edition. 2022. Vol. 61. No. 26.
GOST all authors (up to 50) Copy
Singer F. N., Deacy A. C., Mcguire T. M., Williams C., Buchard A. Chemical Recycling of Poly(Cyclohexene Carbonate) Using a Di‐Mg II Catalyst // Angewandte Chemie - International Edition. 2022. Vol. 61. No. 26.
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RIS Copy
TY - JOUR
DO - 10.1002/anie.202201785
UR - https://doi.org/10.1002/anie.202201785
TI - Chemical Recycling of Poly(Cyclohexene Carbonate) Using a Di‐Mg II Catalyst
T2 - Angewandte Chemie - International Edition
AU - Singer, Frances N
AU - Deacy, Arron C
AU - Mcguire, Thomas M
AU - Williams, Charlotte
AU - Buchard, Antoine
PY - 2022
DA - 2022/05/05
PB - Wiley
IS - 26
VL - 61
PMID - 35442558
SN - 1433-7851
SN - 1521-3773
ER -
BibTex
Cite this
BibTex (up to 50 authors) Copy
@article{2022_Singer,
author = {Frances N Singer and Arron C Deacy and Thomas M Mcguire and Charlotte Williams and Antoine Buchard},
title = {Chemical Recycling of Poly(Cyclohexene Carbonate) Using a Di‐Mg II Catalyst},
journal = {Angewandte Chemie - International Edition},
year = {2022},
volume = {61},
publisher = {Wiley},
month = {may},
url = {https://doi.org/10.1002/anie.202201785},
number = {26},
doi = {10.1002/anie.202201785}
}