Chemische Berichte

, volume 100 , issue 1 , pages 60-70

1.3‐Dipolare Cycloadditionen, XXV. Der Nachweis des freien Diphenylnitrilimins als Zwischenstufe bei Cycloadditionen

James S Clovis ^{1, 2}

Albrecht Eckell ^{1, 2}

Rolf HUISGEN ^{1, 2}

Reiner SUSTMANN ^{1, 2}

Hide authors affiliations Show authors affiliations: 2 affiliations

Institut für Organische Chemie der Universität München |

Research Laboratories Rohm and Haas Comp., Bristol (USA) |

Publication type: Journal Article

Publication date: 1967-01-01

Wiley

Chemische Berichte

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ISSN: 00092940

DOI: 10.1002/cber.19671000108

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Inorganic Chemistry

Abstract

Rasche Folgereaktionen vereitelten bislang die Isolierung substituierter Nitrilimine. Benz-phenylhydrazid-chlorid (3) tauscht nur in Anwesenheit von Triathylamin mit Triathylammoniumchlorid-36Cl das Chlor aus. Identische Orientierungsverhaltnisse bei Cycloadditionen an Zimtsaure-methylester bzw. Crotonsaure-methylester sowie ubereinstimmende Konkurrenzkonstanten bei der Umsetzung mit Dipolarophilen-Paaren beweisen das Auftreten ein und derselben Zwischenstufe bei folgenden Reaktionen: Thermolyse und Photolyse des 2.5-Diphenyl-tetrazols (1), Umsetzungen von Benz-phenylhydrazid-chlorid (3) mit tert. Amin sowie von [α-Nitro-benzyliden]-phenylhydrazin (8) mit Triathylamin und Natriumjodid. Nur das freie Diphenylnitrilimin genugt den strukturellen Anforderungen.

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Clovis J. S. et al. 1.3‐Dipolare Cycloadditionen, XXV. Der Nachweis des freien Diphenylnitrilimins als Zwischenstufe bei Cycloadditionen // Chemische Berichte. 1967. Vol. 100. No. 1. pp. 60-70.

GOST all authors (up to 50) Copy

Clovis J. S., Eckell A., HUISGEN R., SUSTMANN R. 1.3‐Dipolare Cycloadditionen, XXV. Der Nachweis des freien Diphenylnitrilimins als Zwischenstufe bei Cycloadditionen // Chemische Berichte. 1967. Vol. 100. No. 1. pp. 60-70.

RIS |

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RIS Copy

TY - JOUR

DO - 10.1002/cber.19671000108

UR - https://doi.org/10.1002/cber.19671000108

TI - 1.3‐Dipolare Cycloadditionen, XXV. Der Nachweis des freien Diphenylnitrilimins als Zwischenstufe bei Cycloadditionen

T2 - Chemische Berichte

AU - Clovis, James S

AU - Eckell, Albrecht

AU - HUISGEN, Rolf

AU - SUSTMANN, Reiner

PY - 1967

DA - 1967/01/01

PB - Wiley

SP - 60-70

IS - 1

VL - 100

SN - 0009-2940

ER -

BibTex |

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BibTex (up to 50 authors) Copy

@article{1967_Clovis,

author = {James S Clovis and Albrecht Eckell and Rolf HUISGEN and Reiner SUSTMANN},

title = {1.3‐Dipolare Cycloadditionen, XXV. Der Nachweis des freien Diphenylnitrilimins als Zwischenstufe bei Cycloadditionen},

journal = {Chemische Berichte},

year = {1967},

volume = {100},

publisher = {Wiley},

month = {jan},

url = {https://doi.org/10.1002/cber.19671000108},

number = {1},

pages = {60--70},

doi = {10.1002/cber.19671000108}

}

MLA

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MLA Copy

Clovis, James S., et al. “1.3‐Dipolare Cycloadditionen, XXV. Der Nachweis des freien Diphenylnitrilimins als Zwischenstufe bei Cycloadditionen.” Chemische Berichte, vol. 100, no. 1, Jan. 1967, pp. 60-70. https://doi.org/10.1002/cber.19671000108.

Publisher

Wiley

Journal

Chemische Berichte

SJR

—

CiteScore

—

Impact factor

—

ISSN

00092940 (Print)