Heterogeneous Catalysis by Covalent Organic Frameworks (COF): Pd(OAc)2@COF-300 in Cross-Coupling Reactions
Raoni S. Gonçalves
1
,
Alline B V De Oliveira
1
,
Haryadylla C Sindra
1
,
B. S. Archanjo
2
,
Martín E Mendoza
2
,
Leonardo S A Carneiro
3
,
Paulo R.R. Costa
3
,
Pierre Mothé Esteves
1
2
Metrology Materials Division; National Institute of Metrology (Inmetro); Divisão de Metrologia de Materiais; Instituto Nacional de Metrologia, Qualidade e Tecnologia (INMETRO), Duque de Caxias; RJ 25250-020 Brazil
|
Publication type: Journal Article
Publication date: 2016-01-13
scimago Q1
wos Q2
SJR: 0.941
CiteScore: 6.1
Impact factor: 3.9
ISSN: 18673880, 18673899
Catalysis
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
COF-300, an imine-linked, crystalline, and microporous covalent organic framework, modified by coordination of Pd(OAc)2 to its walls, afforded a hybrid material, Pd(OAc)2@COF-300, which was used as an efficient heterogeneous catalyst for cross-coupling reactions. This material showed excellent catalytic activity for the phosphine-free Suzuki–Miyaura, Heck, and Sonogashira cross-coupling reactions with low palladium loadings (0.1 mol % Pd). X-ray photoelectron spectroscopy analysis of the catalyst after the reaction showed that PdII is converted to Pd0, which is trapped within the COFs nanopores. This was confirmed by high-resolution transmission electron microscopy. Moreover, promising results were obtained using Pd(OAc)2@COF-300 under continuous-flow conditions for a Suzuki–Miyaura cross-coupling reaction.
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Gonçalves R. S. et al. Heterogeneous Catalysis by Covalent Organic Frameworks (COF): Pd(OAc)2@COF-300 in Cross-Coupling Reactions // ChemCatChem. 2016. Vol. 8. No. 4. pp. 743-750.
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Gonçalves R. S., De Oliveira A. B. V., Sindra H. C., Archanjo B. S., Mendoza M. E., Carneiro L. S. A., Costa P. R., Esteves P. M. Heterogeneous Catalysis by Covalent Organic Frameworks (COF): Pd(OAc)2@COF-300 in Cross-Coupling Reactions // ChemCatChem. 2016. Vol. 8. No. 4. pp. 743-750.
Cite this
RIS
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TY - JOUR
DO - 10.1002/cctc.201500926
UR - https://doi.org/10.1002/cctc.201500926
TI - Heterogeneous Catalysis by Covalent Organic Frameworks (COF): Pd(OAc)2@COF-300 in Cross-Coupling Reactions
T2 - ChemCatChem
AU - Gonçalves, Raoni S.
AU - De Oliveira, Alline B V
AU - Sindra, Haryadylla C
AU - Archanjo, B. S.
AU - Mendoza, Martín E
AU - Carneiro, Leonardo S A
AU - Costa, Paulo R.R.
AU - Esteves, Pierre Mothé
PY - 2016
DA - 2016/01/13
PB - Wiley
SP - 743-750
IS - 4
VL - 8
SN - 1867-3880
SN - 1867-3899
ER -
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@article{2016_Gonçalves,
author = {Raoni S. Gonçalves and Alline B V De Oliveira and Haryadylla C Sindra and B. S. Archanjo and Martín E Mendoza and Leonardo S A Carneiro and Paulo R.R. Costa and Pierre Mothé Esteves},
title = {Heterogeneous Catalysis by Covalent Organic Frameworks (COF): Pd(OAc)2@COF-300 in Cross-Coupling Reactions},
journal = {ChemCatChem},
year = {2016},
volume = {8},
publisher = {Wiley},
month = {jan},
url = {https://doi.org/10.1002/cctc.201500926},
number = {4},
pages = {743--750},
doi = {10.1002/cctc.201500926}
}
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MLA
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Gonçalves, Raoni S., et al. “Heterogeneous Catalysis by Covalent Organic Frameworks (COF): Pd(OAc)2@COF-300 in Cross-Coupling Reactions.” ChemCatChem, vol. 8, no. 4, Jan. 2016, pp. 743-750. https://doi.org/10.1002/cctc.201500926.