Chemistry - A European Journal

, том 14 , издание 8 , страницы 2420-2434

Remarkable ligand effect in Ni- And Pd-catalyzed bisthiolation and bisselenation of terminal alkynes: Solving the problem of stereoselective dialkyldichalcogenide addition to the C≡C bond

Тип публикации: Journal Article

Дата публикации: 2008-03-07

Wiley

Chemistry - A European Journal

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wos Q2

white level БС1

SJR: 0.981

CiteScore: 6.7

Impact factor: 3.7

ISSN: 09476539, 15213765

DOI: 10.1002/chem.200701278

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PubMed ID: 18213556

General Chemistry

Catalysis

Organic Chemistry

Краткое описание

We have developed two new catalytic systems based on Ni and Pd complexes to solve the challenging problem of dialkyldichalcogenide (Alk2E2; E=S, Se) addition to alkynes. A comparative study of two catalytic systems-Ni/PMe2Ph and Pd/PCy2Ph-has revealed that the Ni catalyst is superior with respect to high catalytic activity and more general scope relative to the Pd system. A novel synthetic methodology was developed for the preparation of (Z)-bis(alkylthio)alkenes and (Z)-bis(alkylseleno)alkenes from terminal alkynes with excellent stereoselectivity and high yields.

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Ananikov V. P. et al. Remarkable ligand effect in Ni- And Pd-catalyzed bisthiolation and bisselenation of terminal alkynes: Solving the problem of stereoselective dialkyldichalcogenide addition to the C≡C bond // Chemistry - A European Journal. 2008. Vol. 14. No. 8. pp. 2420-2434.

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Ananikov V. P., Gayduk K. A., Beletskaya I. P., Khrustalev V. N., Antipin M. Y. Remarkable ligand effect in Ni- And Pd-catalyzed bisthiolation and bisselenation of terminal alkynes: Solving the problem of stereoselective dialkyldichalcogenide addition to the C≡C bond // Chemistry - A European Journal. 2008. Vol. 14. No. 8. pp. 2420-2434.

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TY - JOUR

DO - 10.1002/chem.200701278

UR - https://doi.org/10.1002/chem.200701278

TI - Remarkable ligand effect in Ni- And Pd-catalyzed bisthiolation and bisselenation of terminal alkynes: Solving the problem of stereoselective dialkyldichalcogenide addition to the C≡C bond

T2 - Chemistry - A European Journal

AU - Ananikov, Valentine P

AU - Gayduk, Konstantin A

AU - Beletskaya, Irina P.

AU - Khrustalev, Victor N.

AU - Antipin, Mikhail Yu.

PY - 2008

DA - 2008/03/07

PB - Wiley

SP - 2420-2434

IS - 8

VL - 14

PMID - 18213556

SN - 0947-6539

SN - 1521-3765

ER -

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@article{2008_Ananikov,

author = {Valentine P Ananikov and Konstantin A Gayduk and Irina P. Beletskaya and Victor N. Khrustalev and Mikhail Yu. Antipin},

title = {Remarkable ligand effect in Ni- And Pd-catalyzed bisthiolation and bisselenation of terminal alkynes: Solving the problem of stereoselective dialkyldichalcogenide addition to the C≡C bond},

journal = {Chemistry - A European Journal},

year = {2008},

volume = {14},

publisher = {Wiley},

month = {mar},

url = {https://doi.org/10.1002/chem.200701278},

number = {8},

pages = {2420--2434},

doi = {10.1002/chem.200701278}

}

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Ananikov, Valentine P., et al. “Remarkable ligand effect in Ni- And Pd-catalyzed bisthiolation and bisselenation of terminal alkynes: Solving the problem of stereoselective dialkyldichalcogenide addition to the C≡C bond.” Chemistry - A European Journal, vol. 14, no. 8, Mar. 2008, pp. 2420-2434. https://doi.org/10.1002/chem.200701278.