X‐ray Crystallographic Proof of the Isomer D2‐C84(5) as Trifluoromethylated and Chlorinated Derivatives, C84(CF3)16, C84Cl20, and C84Cl32
Publication type: Journal Article
Publication date: 2012-01-26
scimago Q1
wos Q2
SJR: 0.981
CiteScore: 6.7
Impact factor: 3.7
ISSN: 09476539, 15213765
PubMed ID:
22281723
General Chemistry
Catalysis
Organic Chemistry
Abstract
Minor isomer comes forward: Minor isomer C(84)(5) has been captured by high temperature trifluoromethylation with CF(3)I and chlorination with VCl(4). The compounds C(84)(CF(3))(16), C(84)Cl(20), and C(84)(5)Cl(32) were investigated by X-ray crystallography providing the first direct proof of the cage connectivity of D(2)-C(84)(5). The D(2)-C(84)(5)Cl(32) molecule (see figure; C grey, Cl green) contains two flattened, pyrene-like substructures on opposite poles of the cage resulting in its drum-like shape.
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Total citations:
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Meng Xiangyue 孟. et al. X‐ray Crystallographic Proof of the Isomer D2‐C84(5) as Trifluoromethylated and Chlorinated Derivatives, C84(CF3)16, C84Cl20, and C84Cl32 // Chemistry - A European Journal. 2012. Vol. 18. No. 8. pp. 2217-2220.
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Tamm N. B., Kemnitz E., Troyanov S. X‐ray Crystallographic Proof of the Isomer D2‐C84(5) as Trifluoromethylated and Chlorinated Derivatives, C84(CF3)16, C84Cl20, and C84Cl32 // Chemistry - A European Journal. 2012. Vol. 18. No. 8. pp. 2217-2220.
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TY - JOUR
DO - 10.1002/chem.201103456
UR - https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/chem.201103456
TI - X‐ray Crystallographic Proof of the Isomer D2‐C84(5) as Trifluoromethylated and Chlorinated Derivatives, C84(CF3)16, C84Cl20, and C84Cl32
T2 - Chemistry - A European Journal
AU - Tamm, Nadezhda B
AU - Kemnitz, E.
AU - Troyanov, Sergey
PY - 2012
DA - 2012/01/26
PB - Wiley
SP - 2217-2220
IS - 8
VL - 18
PMID - 22281723
SN - 0947-6539
SN - 1521-3765
ER -
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BibTex (up to 50 authors)
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@article{2012_Meng Xiangyue,
author = {Nadezhda B Tamm and E. Kemnitz and Sergey Troyanov},
title = {X‐ray Crystallographic Proof of the Isomer D2‐C84(5) as Trifluoromethylated and Chlorinated Derivatives, C84(CF3)16, C84Cl20, and C84Cl32},
journal = {Chemistry - A European Journal},
year = {2012},
volume = {18},
publisher = {Wiley},
month = {jan},
url = {https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/chem.201103456},
number = {8},
pages = {2217--2220},
doi = {10.1002/chem.201103456}
}
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Meng Xiangyue, 孟祥月, et al. “X‐ray Crystallographic Proof of the Isomer D2‐C84(5) as Trifluoromethylated and Chlorinated Derivatives, C84(CF3)16, C84Cl20, and C84Cl32.” Chemistry - A European Journal, vol. 18, no. 8, Jan. 2012, pp. 2217-2220. https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/chem.201103456.