volume 2019 issue 23 pages 2819-2829

New Spin-Crossover Complexes of Substituted 2,6-Bis(pyrazol-3-yl)pyridines

Alexander Pavlov 1, 2
Dmitry Yu Aleshin 3, 5
Alexander V Polezhaev 3, 7
Alexander A. Korlyukov 3
Publication typeJournal Article
Publication date2019-05-17
scimago Q2
wos Q3
SJR0.459
CiteScore3.9
Impact factor2.0
ISSN14341948, 10990682
Inorganic Chemistry
Abstract

Here we report two new ligands from a 2,6‐bis(pyrazol‐3‐yl)pyridine family often used in spin‐crossover research and their iron(II) and cobalt(II) complexes with the metal ion trapped in the high‐spin state in solids (according to magnetometry and X‐ray diffraction data). The iron(II) complexes, however, show a gradual spin‐crossover in acetonitrile solution, as probed by the popular Evans method and an analysis of temperature dependent chemical shifts, both rooted in variable‐temperature NMR spectroscopy. The observed stabilization of the high‐spin state by the electron‐withdrawing substituents mirrors the trend previously reported for spin‐crossover iron(II) complexes of isomeric 2,6‐bis(pyrazol‐1‐yl)pyridines.

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Pavlov A. et al. New Spin-Crossover Complexes of Substituted 2,6-Bis(pyrazol-3-yl)pyridines // European Journal of Inorganic Chemistry. 2019. Vol. 2019. No. 23. pp. 2819-2829.
GOST all authors (up to 50) Copy
Pavlov A., Pavlov A. A., Aleshin D. Yu., Nikovskiy I. A., Polezhaev A., Polezhaev A. V., Efimov N. N., Korlyukov A., Korlyukov A. A., Novikov V. V., Nelyubina Y. V. New Spin-Crossover Complexes of Substituted 2,6-Bis(pyrazol-3-yl)pyridines // European Journal of Inorganic Chemistry. 2019. Vol. 2019. No. 23. pp. 2819-2829.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1002/ejic.201900432
UR - https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201900432
TI - New Spin-Crossover Complexes of Substituted 2,6-Bis(pyrazol-3-yl)pyridines
T2 - European Journal of Inorganic Chemistry
AU - Pavlov, Alexander
AU - Pavlov, Alexander A.
AU - Aleshin, Dmitry Yu
AU - Nikovskiy, Igor A
AU - Polezhaev, Alexander
AU - Polezhaev, Alexander V
AU - Efimov, Nikolay N.
AU - Korlyukov, Alexander
AU - Korlyukov, Alexander A.
AU - Novikov, Valentin V
AU - Nelyubina, Yulia V.
PY - 2019
DA - 2019/05/17
PB - Wiley
SP - 2819-2829
IS - 23
VL - 2019
SN - 1434-1948
SN - 1099-0682
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2019_Pavlov,
author = {Alexander Pavlov and Alexander A. Pavlov and Dmitry Yu Aleshin and Igor A Nikovskiy and Alexander Polezhaev and Alexander V Polezhaev and Nikolay N. Efimov and Alexander Korlyukov and Alexander A. Korlyukov and Valentin V Novikov and Yulia V. Nelyubina},
title = {New Spin-Crossover Complexes of Substituted 2,6-Bis(pyrazol-3-yl)pyridines},
journal = {European Journal of Inorganic Chemistry},
year = {2019},
volume = {2019},
publisher = {Wiley},
month = {may},
url = {https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201900432},
number = {23},
pages = {2819--2829},
doi = {10.1002/ejic.201900432}
}
MLA
Cite this
MLA Copy
Pavlov, Alexander, et al. “New Spin-Crossover Complexes of Substituted 2,6-Bis(pyrazol-3-yl)pyridines.” European Journal of Inorganic Chemistry, vol. 2019, no. 23, May. 2019, pp. 2819-2829. https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201900432.