Synthesis of Chlorinated Biphenyls by Suzuki Cross‐Coupling Using Diamine or Diimine‐Palladium Complexes
Тип публикации: Journal Article
Дата публикации: 2008-07-29
scimago Q2
wos Q2
БС2
SJR: 0.558
CiteScore: 4.3
Impact factor: 2.7
ISSN: 1434193X, 10990690
Organic Chemistry
Physical and Theoretical Chemistry
Краткое описание
Several novel diimines (Salen‐type ligands) 2a–2i and their reduced diamine counterparts 3b,3d–3g and 3i form complexes 4a–4i, 5b,5d–5g, and 5i with PdCl2 in DMF or methanol. Using 1 mol‐% of the isolated complexes 4e and 5f many polychlorinated biphenyls (PCBs) can be prepared in moderate to excellent yields according to the Suzuki cross‐coupling protocol with contact to air. Several 4‐acetylbiphenyls prepared by this method can be converted in moderate yields into the corresponding biphenylcarboxylic acids (BCAs) by alkaline cleavage. An X‐ray crystal structure determination confirms the structure of complex 5f.(© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2008)
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Kylmälä T. et al. Synthesis of Chlorinated Biphenyls by Suzuki Cross‐Coupling Using Diamine or Diimine‐Palladium Complexes // European Journal of Organic Chemistry. 2008. Vol. 2008. No. 23. pp. 4019-4024.
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Kylmälä T., Kuuloja N., Xu Y., Rissanen K., Franzén R. Synthesis of Chlorinated Biphenyls by Suzuki Cross‐Coupling Using Diamine or Diimine‐Palladium Complexes // European Journal of Organic Chemistry. 2008. Vol. 2008. No. 23. pp. 4019-4024.
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TY - JOUR
DO - 10.1002/ejoc.200800119
UR - https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejoc.200800119
TI - Synthesis of Chlorinated Biphenyls by Suzuki Cross‐Coupling Using Diamine or Diimine‐Palladium Complexes
T2 - European Journal of Organic Chemistry
AU - Kylmälä, Tuula
AU - Kuuloja, Noora
AU - Xu, Youjun
AU - Rissanen, Kari
AU - Franzén, Robert
PY - 2008
DA - 2008/07/29
PB - Wiley
SP - 4019-4024
IS - 23
VL - 2008
SN - 1434-193X
SN - 1099-0690
ER -
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@article{2008_Kylmälä,
author = {Tuula Kylmälä and Noora Kuuloja and Youjun Xu and Kari Rissanen and Robert Franzén},
title = {Synthesis of Chlorinated Biphenyls by Suzuki Cross‐Coupling Using Diamine or Diimine‐Palladium Complexes},
journal = {European Journal of Organic Chemistry},
year = {2008},
volume = {2008},
publisher = {Wiley},
month = {jul},
url = {https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejoc.200800119},
number = {23},
pages = {4019--4024},
doi = {10.1002/ejoc.200800119}
}
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MLA
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Kylmälä, Tuula, et al. “Synthesis of Chlorinated Biphenyls by Suzuki Cross‐Coupling Using Diamine or Diimine‐Palladium Complexes.” European Journal of Organic Chemistry, vol. 2008, no. 23, Jul. 2008, pp. 4019-4024. https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejoc.200800119.