volume 2017 issue 19 pages 2836-2841

Synthetic Route to 4,4a- and 3,4-Dihydroxanthones through [4+2] Cycloaddition and Base-Assisted Sigmatropic Rearrangement

R V Shutov 1
Nikolay N Kuzmich 3, 4
Alexander V. Belyakov 5
Publication typeJournal Article
Publication date2017-05-18
scimago Q2
wos Q2
SJR0.558
CiteScore4.3
Impact factor2.7
ISSN1434193X, 10990690
Organic Chemistry
Physical and Theoretical Chemistry
Abstract

The [4+2] cycloaddition of chromone‐fused dienes with enamines was found to be an efficient method for the synthesis of 4,4a‐ and 3,4‐dihydroxanthone derivatives. Either product type could be obtained by choosing the proper conditions [reaction time and addition of La(NO3)3 as a Lewis acid]. Calculations using density functional theory and Møller–Plesset perturbation theory showed that the isomerization of 4,4a‐dihydroxanthones to 3,4‐dihydroxanthones occurred through a base‐assisted sigmatropic rearrangement. The described reaction provides a convenient route to a natural‐product‐inspired group of 4,4a‐dihydroxanthones with cytotoxic activity.

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GOST |
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GOST Copy
Chernov N. M. et al. Synthetic Route to 4,4a- and 3,4-Dihydroxanthones through [4+2] Cycloaddition and Base-Assisted Sigmatropic Rearrangement // European Journal of Organic Chemistry. 2017. Vol. 2017. No. 19. pp. 2836-2841.
GOST all authors (up to 50) Copy
Chernov N. M., Shutov R. V., Sharoyko V., Kuzmich N. N., Belyakov A. V., Yakovlev I. P. Synthetic Route to 4,4a- and 3,4-Dihydroxanthones through [4+2] Cycloaddition and Base-Assisted Sigmatropic Rearrangement // European Journal of Organic Chemistry. 2017. Vol. 2017. No. 19. pp. 2836-2841.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1002/ejoc.201700310
UR - https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejoc.201700310
TI - Synthetic Route to 4,4a- and 3,4-Dihydroxanthones through [4+2] Cycloaddition and Base-Assisted Sigmatropic Rearrangement
T2 - European Journal of Organic Chemistry
AU - Chernov, Nikita M
AU - Shutov, R V
AU - Sharoyko, Vladimir
AU - Kuzmich, Nikolay N
AU - Belyakov, Alexander V.
AU - Yakovlev, Igor P
PY - 2017
DA - 2017/05/18
PB - Wiley
SP - 2836-2841
IS - 19
VL - 2017
SN - 1434-193X
SN - 1099-0690
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2017_Chernov,
author = {Nikita M Chernov and R V Shutov and Vladimir Sharoyko and Nikolay N Kuzmich and Alexander V. Belyakov and Igor P Yakovlev},
title = {Synthetic Route to 4,4a- and 3,4-Dihydroxanthones through [4+2] Cycloaddition and Base-Assisted Sigmatropic Rearrangement},
journal = {European Journal of Organic Chemistry},
year = {2017},
volume = {2017},
publisher = {Wiley},
month = {may},
url = {https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejoc.201700310},
number = {19},
pages = {2836--2841},
doi = {10.1002/ejoc.201700310}
}
MLA
Cite this
MLA Copy
Chernov, Nikita M., et al. “Synthetic Route to 4,4a- and 3,4-Dihydroxanthones through [4+2] Cycloaddition and Base-Assisted Sigmatropic Rearrangement.” European Journal of Organic Chemistry, vol. 2017, no. 19, May. 2017, pp. 2836-2841. https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejoc.201700310.