Optimized reaction conditions for the cross-metathesis of methyl oleate and oleylamine with ethyl acrylate
Publication type: Journal Article
Publication date: 2012-01-24
scimago Q3
wos Q3
SJR: 0.321
CiteScore: 3.4
Impact factor: 1.9
ISSN: 00269247, 14344475
General Chemistry
Abstract
The cross-metathesis of methyl oleate and oleylamine with ethyl acrylate has been studied using three different ruthenium-based second-generation catalysts. Emphasis was on determining the smallest amount of catalyst necessary for full conversion of technical grade educts. Conversion of methyl oleate is best performed in the presence of 10 equiv. ethyl acrylate without use of additional solvent whereas oleylamine cannot be used directly and protection of the amino group is necessary. An easy protection procedure for oleylamine with acetic anhydride was developed and the best results for cross-metathesis of N-acetyloleylamine were obtained in toluene solution. .
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GOST
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Abbas M., Slugovc C. Optimized reaction conditions for the cross-metathesis of methyl oleate and oleylamine with ethyl acrylate // Monatshefte fur Chemie. 2012. Vol. 143. No. 4. pp. 669-673.
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Abbas M., Slugovc C. Optimized reaction conditions for the cross-metathesis of methyl oleate and oleylamine with ethyl acrylate // Monatshefte fur Chemie. 2012. Vol. 143. No. 4. pp. 669-673.
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RIS
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TY - JOUR
DO - 10.1007/s00706-011-0717-x
UR - https://doi.org/10.1007/s00706-011-0717-x
TI - Optimized reaction conditions for the cross-metathesis of methyl oleate and oleylamine with ethyl acrylate
T2 - Monatshefte fur Chemie
AU - Abbas, Mudassar
AU - Slugovc, Christian
PY - 2012
DA - 2012/01/24
PB - Springer Nature
SP - 669-673
IS - 4
VL - 143
SN - 0026-9247
SN - 1434-4475
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2012_Abbas,
author = {Mudassar Abbas and Christian Slugovc},
title = {Optimized reaction conditions for the cross-metathesis of methyl oleate and oleylamine with ethyl acrylate},
journal = {Monatshefte fur Chemie},
year = {2012},
volume = {143},
publisher = {Springer Nature},
month = {jan},
url = {https://doi.org/10.1007/s00706-011-0717-x},
number = {4},
pages = {669--673},
doi = {10.1007/s00706-011-0717-x}
}
Cite this
MLA
Copy
Abbas, Mudassar, and Christian Slugovc. “Optimized reaction conditions for the cross-metathesis of methyl oleate and oleylamine with ethyl acrylate.” Monatshefte fur Chemie, vol. 143, no. 4, Jan. 2012, pp. 669-673. https://doi.org/10.1007/s00706-011-0717-x.