N-[2,2-Bis(methoxy-NNO-azoxy)ethyl]pyrazoles
Publication type: Journal Article
Publication date: 2017-06-01
scimago Q4
wos Q4
SJR: 0.243
CiteScore: 2.7
Impact factor: 1.0
ISSN: 00093122, 15738353
Organic Chemistry
Abstract
The reaction of 2,2-bis(methoxy-NNO-azoxy)ethanol nitrate with pyrazole, 3-nitropyrazole, 4-nitropyrazole, or 3,4-dinitropyrazole allowed to obtain the respective N-[2,2-bis(methoxy-NNO-azoxy)ethyl]pyrazoles. In the case of 3-nitropyrazole, only the 3-nitro isomer was formed, while alkylation of 3,4-dinitropyrazole led to a mixture of 3,4- and 4,5-dinitro isomers in 7:1 ratio, which was difficult to separate. The obtained pyrazoles were characterized by 1H, 13C, and 15N NMR spectroscopy. X-ray structural studies were performed for the synthesized 3-NO2, 4-NO2, and 3,4-(NO2)2 derivatives.
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Zyuzin I. N., Suponitsky K. Yu., Dalinger I. L. N-[2,2-Bis(methoxy-NNO-azoxy)ethyl]pyrazoles // Chemistry of Heterocyclic Compounds. 2017. Vol. 53. No. 6-7. pp. 702-709.
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Zyuzin I. N., Suponitsky K. Yu., Dalinger I. L. N-[2,2-Bis(methoxy-NNO-azoxy)ethyl]pyrazoles // Chemistry of Heterocyclic Compounds. 2017. Vol. 53. No. 6-7. pp. 702-709.
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RIS
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TY - JOUR
DO - 10.1007/s10593-017-2112-y
UR - https://doi.org/10.1007/s10593-017-2112-y
TI - N-[2,2-Bis(methoxy-NNO-azoxy)ethyl]pyrazoles
T2 - Chemistry of Heterocyclic Compounds
AU - Zyuzin, Igor N
AU - Suponitsky, Kirill Yu
AU - Dalinger, Igor L
PY - 2017
DA - 2017/06/01
PB - Springer Nature
SP - 702-709
IS - 6-7
VL - 53
SN - 0009-3122
SN - 1573-8353
ER -
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BibTex (up to 50 authors)
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@article{2017_Zyuzin,
author = {Igor N Zyuzin and Kirill Yu Suponitsky and Igor L Dalinger},
title = {N-[2,2-Bis(methoxy-NNO-azoxy)ethyl]pyrazoles},
journal = {Chemistry of Heterocyclic Compounds},
year = {2017},
volume = {53},
publisher = {Springer Nature},
month = {jun},
url = {https://doi.org/10.1007/s10593-017-2112-y},
number = {6-7},
pages = {702--709},
doi = {10.1007/s10593-017-2112-y}
}
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MLA
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Zyuzin, Igor N., et al. “N-[2,2-Bis(methoxy-NNO-azoxy)ethyl]pyrazoles.” Chemistry of Heterocyclic Compounds, vol. 53, no. 6-7, Jun. 2017, pp. 702-709. https://doi.org/10.1007/s10593-017-2112-y.