Journal of Thermal Analysis and Calorimetry, volume 147, issue 15, pages 8235-8242
Cocrystals of betulin with adipic acid: preparation and thermal behavior
Myz S A
1
,
Mikhailenko M A
1
,
Mikhailovskaya A V
1
,
Bulina N.V.
1
,
Gerasimov K.B
1
,
Politov A.A
1, 2
,
Kuznetsova S.A
3
,
Publication type: Journal Article
Publication date: 2021-11-21
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor: 4.4
ISSN: 13886150, 15882926, 03684466, 15728943
Physical and Theoretical Chemistry
Condensed Matter Physics
Abstract
The cocrystal of betulin (BE) with adipic acid (AA) was prepared using a liquid-assisted grinding method. The formation of BE-AA cocrystal was confirmed by powder X-ray diffraction, IR spectroscopy and thermal analysis methods. It was assumed that 1:1 BE-AA cocrystal hydrate was formed when liquid-assisted grinding was carried out using water-miscible liquids in which the solubility of adipic acid was higher than in others. The cocrystal hydrate was stable under room temperature and rather high relative humidity. Nevertheless, the betulin–adipic acid cocrystal was found to decompose under heating after the loss of water molecules, followed by phase transformation. An anhydrous BE-AA cocrystal was also prepared by the BE-AA physical mixture heating up to the point of adipic acid melting.
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Springer Nature
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Myz S. A. et al. Cocrystals of betulin with adipic acid: preparation and thermal behavior // Journal of Thermal Analysis and Calorimetry. 2021. Vol. 147. No. 15. pp. 8235-8242.
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Myz S. A., Mikhailenko M. A., Mikhailovskaya A. V., Bulina N., Gerasimov K., Politov A., Kuznetsova S., Shakhtshneider T. Cocrystals of betulin with adipic acid: preparation and thermal behavior // Journal of Thermal Analysis and Calorimetry. 2021. Vol. 147. No. 15. pp. 8235-8242.
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TY - JOUR
DO - 10.1007/s10973-021-11107-4
UR - https://doi.org/10.1007%2Fs10973-021-11107-4
TI - Cocrystals of betulin with adipic acid: preparation and thermal behavior
T2 - Journal of Thermal Analysis and Calorimetry
AU - Myz, S A
AU - Mikhailenko, M A
AU - Mikhailovskaya, A V
AU - Bulina, N.V.
AU - Gerasimov, K.B
AU - Politov, A.A
AU - Kuznetsova, S.A
AU - Shakhtshneider, Tatyana
PY - 2021
DA - 2021/11/21 00:00:00
PB - Springer Nature
SP - 8235-8242
IS - 15
VL - 147
SN - 1388-6150
SN - 1588-2926
SN - 0368-4466
SN - 1572-8943
ER -
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@article{2021_Myz,
author = {S A Myz and M A Mikhailenko and A V Mikhailovskaya and N.V. Bulina and K.B Gerasimov and A.A Politov and S.A Kuznetsova and Tatyana Shakhtshneider},
title = {Cocrystals of betulin with adipic acid: preparation and thermal behavior},
journal = {Journal of Thermal Analysis and Calorimetry},
year = {2021},
volume = {147},
publisher = {Springer Nature},
month = {nov},
url = {https://doi.org/10.1007%2Fs10973-021-11107-4},
number = {15},
pages = {8235--8242},
doi = {10.1007/s10973-021-11107-4}
}
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Myz, S. A., et al. “Cocrystals of betulin with adipic acid: preparation and thermal behavior.” Journal of Thermal Analysis and Calorimetry, vol. 147, no. 15, Nov. 2021, pp. 8235-8242. https://doi.org/10.1007%2Fs10973-021-11107-4.
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