Springer Nature
Russian Chemical Bulletin
,  volume 56 ,  issue 2 ,  pages 271-275

Synthesis and thermal decomposition of hydrotrioxide obtained by ozonization of exo-bicyclo[2.2.1]heptan-2-ol

Publication type: Journal Article
Publication date: 2007-02-01
Springer Nature
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
Low-temperature (−70 °C) ozonization of exo-bicyclo[2.2.1]heptan-2-ol in CCl3F led to a hydrotrioxide, which was identified by 1H NMR spectroscopy. Kinetics of decomposition of given hydrotrioxide was studied by analysis of the chemiluminescence fading in the IR range of the spectrum and the activation parameters of the process were calculated. Singlet oxygen (1Δg) served as an emitter of eradiation. Yields of 1O2 in a range of temperature from −31.0 to +12.5 °C were determined (at −31 °C the yield was 37.6%). Bicyclo[2.2.1]heptan-2-one was found to be the main product of decomposition of the hydrotrioxide (the yield was 98%).
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GOST Copy
Abdrakhmanova A. R. et al. Synthesis and thermal decomposition of hydrotrioxide obtained by ozonization of exo-bicyclo[2.2.1]heptan-2-ol // Russian Chemical Bulletin. 2007. Vol. 56. No. 2. pp. 271-275.
GOST all authors (up to 50) Copy
Abdrakhmanova A. R., Khalitova L. R., Spirikhin L. V., Dokichev V. A., Grabovskiy S. A., Kabalnova N. N. Synthesis and thermal decomposition of hydrotrioxide obtained by ozonization of exo-bicyclo[2.2.1]heptan-2-ol // Russian Chemical Bulletin. 2007. Vol. 56. No. 2. pp. 271-275.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1007/s11172-007-0044-x
UR - https://doi.org/10.1007/s11172-007-0044-x
TI - Synthesis and thermal decomposition of hydrotrioxide obtained by ozonization of exo-bicyclo[2.2.1]heptan-2-ol
T2 - Russian Chemical Bulletin
AU - Abdrakhmanova, A R
AU - Khalitova, L R
AU - Spirikhin, L V
AU - Dokichev, V A
AU - Grabovskiy, S A
AU - Kabalnova, N N
PY - 2007
DA - 2007/02/01
PB - Springer Nature
SP - 271-275
IS - 2
VL - 56
SN - 1066-5285
SN - 1573-9171
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2007_Abdrakhmanova,
author = {A R Abdrakhmanova and L R Khalitova and L V Spirikhin and V A Dokichev and S A Grabovskiy and N N Kabalnova},
title = {Synthesis and thermal decomposition of hydrotrioxide obtained by ozonization of exo-bicyclo[2.2.1]heptan-2-ol},
journal = {Russian Chemical Bulletin},
year = {2007},
volume = {56},
publisher = {Springer Nature},
month = {feb},
url = {https://doi.org/10.1007/s11172-007-0044-x},
number = {2},
pages = {271--275},
doi = {10.1007/s11172-007-0044-x}
}
MLA
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MLA Copy
Abdrakhmanova, A. R., et al. “Synthesis and thermal decomposition of hydrotrioxide obtained by ozonization of exo-bicyclo[2.2.1]heptan-2-ol.” Russian Chemical Bulletin, vol. 56, no. 2, Feb. 2007, pp. 271-275. https://doi.org/10.1007/s11172-007-0044-x.