том 21 издание 4 страницы 459-462

Preparation and X-ray structure of [H3O+�18-crown-6]-[(H5O 2 + )(Cl?)2], a compound containing both H3O+ and H5O 2 + crystallized from aromatic solution

Тип публикацииJournal Article
Дата публикации1991-08-01
scimago Q3
wos Q4
БС3
SJR0.209
CiteScore2
Impact factor0.6
ISSN10741542, 15728854
General Chemistry
Spectroscopy
Structural Biology
Condensed Matter Physics
Краткое описание
The title compound was synthesized by the reaction of [H3O+·18-crown-6][Cl-H-Cl−]·3.8 C6H5Me with two equivalents of H2O. Colorless crystals, which slowly deposited from the corresponding liquid clathrate, belong to the monoclinic space group P21/n witha=10.648(6),b=9.571(2),c=20.801(6) Å,β=98.67(5)°, andD c=1.24 g cm−3 forZ=4. Refinement based on 1609 observed reflections led to a finalR value of 0.072. In the crystal structure the [H3O+·18-crown-6]+ cations are packed in layers separated by puckered sheets of [(H5O 2 + )(Cl−)2]−.
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Atwood J. L. et al. Preparation and X-ray structure of [H3O+�18-crown-6]-[(H5O 2 + )(Cl?)2], a compound containing both H3O+ and H5O 2 + crystallized from aromatic solution // Journal of Chemical Crystallography. 1991. Vol. 21. No. 4. pp. 459-462.
ГОСТ со всеми авторами (до 50) Скопировать
Atwood J. L., Bott S. G., Robinson K. D., Bishop E. J., MAY M. T. Preparation and X-ray structure of [H3O+�18-crown-6]-[(H5O 2 + )(Cl?)2], a compound containing both H3O+ and H5O 2 + crystallized from aromatic solution // Journal of Chemical Crystallography. 1991. Vol. 21. No. 4. pp. 459-462.
RIS |
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TY - JOUR
DO - 10.1007/bf01160659
UR - https://doi.org/10.1007/bf01160659
TI - Preparation and X-ray structure of [H3O+�18-crown-6]-[(H5O 2 + )(Cl?)2], a compound containing both H3O+ and H5O 2 + crystallized from aromatic solution
T2 - Journal of Chemical Crystallography
AU - Atwood, Jerry L.
AU - Bott, Simon G.
AU - Robinson, Kerry D
AU - Bishop, Elizabeth J
AU - MAY, MICHAEL T.
PY - 1991
DA - 1991/08/01
PB - Springer Nature
SP - 459-462
IS - 4
VL - 21
SN - 1074-1542
SN - 1572-8854
ER -
BibTex |
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BibTex (до 50 авторов) Скопировать
@article{1991_Atwood,
author = {Jerry L. Atwood and Simon G. Bott and Kerry D Robinson and Elizabeth J Bishop and MICHAEL T. MAY},
title = {Preparation and X-ray structure of [H3O+�18-crown-6]-[(H5O 2 + )(Cl?)2], a compound containing both H3O+ and H5O 2 + crystallized from aromatic solution},
journal = {Journal of Chemical Crystallography},
year = {1991},
volume = {21},
publisher = {Springer Nature},
month = {aug},
url = {https://doi.org/10.1007/bf01160659},
number = {4},
pages = {459--462},
doi = {10.1007/bf01160659}
}
MLA
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Atwood, Jerry L., et al. “Preparation and X-ray structure of [H3O+�18-crown-6]-[(H5O 2 + )(Cl?)2], a compound containing both H3O+ and H5O 2 + crystallized from aromatic solution.” Journal of Chemical Crystallography, vol. 21, no. 4, Aug. 1991, pp. 459-462. https://doi.org/10.1007/bf01160659.