The role of pH in the synthesis of diaziridines 2. The effect of pH on the synthesis of diaziridines from amines, carbonyl compounds and NaOCl
Publication type: Journal Article
Publication date: 1997-07-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
In the synthesis of diaziridines from amines, carbonyl compounds, and NaOCl in water, the yields of 1,2-dialkyldiaziridines and of 1,2,3-trisubstituted diaziridines prepared from amines with electron-withdrawing substituents in the side chain are less sensitive to changes in pH than the yields of 1,2,3-trialkyldiaziridines with simple alkyl substituents. The formation of 1,5-diazabicyclo[3.1.0]hexanes is insensitive to the pH in 6.5–13.0 range. This difference is explained by the occurrence of two competing pathways to the key intermediate,N-chloroaminal.
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Kuznetsov V. V., Makhova N. N., Khmelnitskii L. I. The role of pH in the synthesis of diaziridines 2. The effect of pH on the synthesis of diaziridines from amines, carbonyl compounds and NaOCl // Russian Chemical Bulletin. 1997. Vol. 46. No. 7. pp. 1354-1356.
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Kuznetsov V. V., Makhova N. N., Khmelnitskii L. I. The role of pH in the synthesis of diaziridines 2. The effect of pH on the synthesis of diaziridines from amines, carbonyl compounds and NaOCl // Russian Chemical Bulletin. 1997. Vol. 46. No. 7. pp. 1354-1356.
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TY - JOUR
DO - 10.1007/BF02495943
UR - https://doi.org/10.1007/BF02495943
TI - The role of pH in the synthesis of diaziridines 2. The effect of pH on the synthesis of diaziridines from amines, carbonyl compounds and NaOCl
T2 - Russian Chemical Bulletin
AU - Kuznetsov, V. V.
AU - Makhova, N N
AU - Khmelnitskii, L. I.
PY - 1997
DA - 1997/07/01
PB - Springer Nature
SP - 1354-1356
IS - 7
VL - 46
SN - 1066-5285
SN - 1573-9171
ER -
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BibTex (up to 50 authors)
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@article{1997_Kuznetsov,
author = {V. V. Kuznetsov and N N Makhova and L. I. Khmelnitskii},
title = {The role of pH in the synthesis of diaziridines 2. The effect of pH on the synthesis of diaziridines from amines, carbonyl compounds and NaOCl},
journal = {Russian Chemical Bulletin},
year = {1997},
volume = {46},
publisher = {Springer Nature},
month = {jul},
url = {https://doi.org/10.1007/BF02495943},
number = {7},
pages = {1354--1356},
doi = {10.1007/BF02495943}
}
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MLA
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Kuznetsov, V. V., et al. “The role of pH in the synthesis of diaziridines 2. The effect of pH on the synthesis of diaziridines from amines, carbonyl compounds and NaOCl.” Russian Chemical Bulletin, vol. 46, no. 7, Jul. 1997, pp. 1354-1356. https://doi.org/10.1007/BF02495943.