Pivalate bridged high spin manganese(II) and iron(II) polymers
I. L. Eremenko
1
,
M. A. Kiskin
1
,
I.G. Fomina
1
,
A. A. Sidorov
1
,
G.G. Aleksandrov
1
,
V. N. Ikorskii
2
,
Yu G Shvedenkov
2
,
Yu.V. Rakitin
1
,
V. M. Novotortsev
1
Тип публикации: Journal Article
Дата публикации: 2005-09-01
scimago Q2
wos Q1
БС1
SJR: 0.515
CiteScore: 6.7
Impact factor: 3.6
ISSN: 10407278, 15728862
General Chemistry
Biochemistry
Condensed Matter Physics
General Materials Science
Краткое описание
Antiferromagnetic Mn(II) polymers of general formula {[L2Mn(μ-OOCCMe3)2][Mn2(μ-OOCCMe3)4]}n (L = 1,2-phenylenediamine (3) and 4,5-dimethyl-1,2-phenylenediamine (4)) were synthesized from [Mn(μ-OOCCMe3)2(HOEt)] n (1) polymer and arenediamines in MeCN solution. The tetranuclear cluster Fe4(μ3-OH)2(μ-OOCCMe3)4(η2-OOCCMe3)2(EtOH)6 (5) was prepared by reacting FeSO4·7H2O with KOOCCMe3 in EtOH and was used as starting pivalate iron(II) agent in further reactions. The thermolysis of 5 in MeCN was shown to result in a ferromagnetic polymer [Fe(μ-OOCCMe3)2] n (6) containing tetrahedral iron(II) atoms. Cluster 5 was found to react with o-phenylenediamine giving rise to ferrimagnetic polymer [Fe(μ-OOCCMe3)2(HOEt)]n (7). The reaction 7 with 2,6-diaminopyridine in MeCN results in binuclear antiferromagnetic complex (2,6-(NH2)2C5H3N)2Fe2(μ-OOCCMe3)4· 4MeCN (8). However the reaction of 4,5-dimethyl-1,2-phenylenediamine with polymer 7 yields a polymer {[L2Fe(μ-OOCCMe3)2][Fe2 (μ-OOCCMe3)4]} n (9), which is an analogue of the manganese polymer 4. All newly synthesized compounds were characterized by the by X-ray diffraction studies and magnetic measurement.
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Eremenko I. L. et al. Pivalate bridged high spin manganese(II) and iron(II) polymers // Journal of Cluster Science. 2005. Vol. 16. No. 3. pp. 331-351.
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Eremenko I. L., Kiskin M. A., Fomina I., Sidorov A. A., Aleksandrov G., Ikorskii V. N., Shvedenkov Yu. G., Rakitin Y., Novotortsev V. M. Pivalate bridged high spin manganese(II) and iron(II) polymers // Journal of Cluster Science. 2005. Vol. 16. No. 3. pp. 331-351.
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TY - JOUR
DO - 10.1007/s10876-005-0009-x
UR - https://doi.org/10.1007/s10876-005-0009-x
TI - Pivalate bridged high spin manganese(II) and iron(II) polymers
T2 - Journal of Cluster Science
AU - Eremenko, I. L.
AU - Kiskin, M. A.
AU - Fomina, I.G.
AU - Sidorov, A. A.
AU - Aleksandrov, G.G.
AU - Ikorskii, V. N.
AU - Shvedenkov, Yu G
AU - Rakitin, Yu.V.
AU - Novotortsev, V. M.
PY - 2005
DA - 2005/09/01
PB - Springer Nature
SP - 331-351
IS - 3
VL - 16
SN - 1040-7278
SN - 1572-8862
ER -
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@article{2005_Eremenko,
author = {I. L. Eremenko and M. A. Kiskin and I.G. Fomina and A. A. Sidorov and G.G. Aleksandrov and V. N. Ikorskii and Yu G Shvedenkov and Yu.V. Rakitin and V. M. Novotortsev},
title = {Pivalate bridged high spin manganese(II) and iron(II) polymers},
journal = {Journal of Cluster Science},
year = {2005},
volume = {16},
publisher = {Springer Nature},
month = {sep},
url = {https://doi.org/10.1007/s10876-005-0009-x},
number = {3},
pages = {331--351},
doi = {10.1007/s10876-005-0009-x}
}
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MLA
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Eremenko, I. L., et al. “Pivalate bridged high spin manganese(II) and iron(II) polymers.” Journal of Cluster Science, vol. 16, no. 3, Sep. 2005, pp. 331-351. https://doi.org/10.1007/s10876-005-0009-x.