1,1-Cyclohexanediacetate as New Bridging Ligand for Assembling of Homo- and Heterometallic Molecular Complexes with Cu 3 II , Cu 2 II Ln 2 III (Ln = Sm or Gd) and Ni 2 II Gd 2 III Cores: Synthesis, Structure and Magnetic Properties
Natalya Gogoleva
1
,
Ekaterina Zorina Tikhonova
1
,
Grigory Aleksandrov
1
,
Anatoly Lermontov
1
,
Nikolay Efimov
1
,
Artem Bogomyakov
2
,
Elena Ugolkova
1
,
Sergey Kolotilov
3
,
Aleksey Sidorov
1
,
Vadim Minin
1
,
Vladimir Novotortsev
1
,
3
L. V. Pisarzhevskii Institute of Physical Chemistry of the National Academy of Sciences of the Ukraine, Kiev, Ukraine
|
Publication type: Journal Article
Publication date: 2014-06-08
scimago Q2
wos Q1
SJR: 0.515
CiteScore: 6.7
Impact factor: 3.6
ISSN: 10407278, 15728862
General Chemistry
Biochemistry
Condensed Matter Physics
General Materials Science
Abstract
Interaction of [Cu2(Piv)4(HPiv)2] (Piv− = pivalate) with tetrabutylammonium salt of 1,1-cyclohexanediacetate (Chda2−) and 2,2-bipyridine (2,2′-bpy) in acetonitrile led to formation of the trinuclear homometallic complex [Cu3(2,2′-bpy)2(Chda)2(Piv)2]·2MeCN·0.4H2O (1·2MeCN·0.4H2O). In similar conditions but in presence of [Ln2(Piv)6(HPiv)7] tetranuclear heterometallic complexes [Ln2IIICu2II(2,2′-bpy)2(Chda)2(Piv)6] (Ln = SmIII, 2·2MeCN, or GdIII, 3·2MeCN·5H2O) and [Gd2IIINi2II(2,2′-bpy)2(Chda)2(Piv)6] (4) were synthesized. Carboxylic groups in Piv− and Chda2− act as bridges between the metal ions in all complexes. Temperature dependencies of magnetic susceptibilities and room-temperature solid-state ESR spectra of compounds 2·2MeCN, 3·2MeCN·5H2O, 4 were studied and analyzed.
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Gogoleva N. et al. 1,1-Cyclohexanediacetate as New Bridging Ligand for Assembling of Homo- and Heterometallic Molecular Complexes with Cu 3 II , Cu 2 II Ln 2 III (Ln = Sm or Gd) and Ni 2 II Gd 2 III Cores: Synthesis, Structure and Magnetic Properties // Journal of Cluster Science. 2014. Vol. 26. No. 1. pp. 137-155.
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Gogoleva N., Zorina Tikhonova E., Aleksandrov G., Lermontov A., Efimov N., Bogomyakov A., Ugolkova E., Kolotilov S., Sidorov A., Minin V., Novotortsev V., Eremenko I. 1,1-Cyclohexanediacetate as New Bridging Ligand for Assembling of Homo- and Heterometallic Molecular Complexes with Cu 3 II , Cu 2 II Ln 2 III (Ln = Sm or Gd) and Ni 2 II Gd 2 III Cores: Synthesis, Structure and Magnetic Properties // Journal of Cluster Science. 2014. Vol. 26. No. 1. pp. 137-155.
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TY - JOUR
DO - 10.1007/s10876-014-0740-2
UR - https://doi.org/10.1007/s10876-014-0740-2
TI - 1,1-Cyclohexanediacetate as New Bridging Ligand for Assembling of Homo- and Heterometallic Molecular Complexes with Cu 3 II , Cu 2 II Ln 2 III (Ln = Sm or Gd) and Ni 2 II Gd 2 III Cores: Synthesis, Structure and Magnetic Properties
T2 - Journal of Cluster Science
AU - Gogoleva, Natalya
AU - Zorina Tikhonova, Ekaterina
AU - Aleksandrov, Grigory
AU - Lermontov, Anatoly
AU - Efimov, Nikolay
AU - Bogomyakov, Artem
AU - Ugolkova, Elena
AU - Kolotilov, Sergey
AU - Sidorov, Aleksey
AU - Minin, Vadim
AU - Novotortsev, Vladimir
AU - Eremenko, Igor
PY - 2014
DA - 2014/06/08
PB - Springer Nature
SP - 137-155
IS - 1
VL - 26
SN - 1040-7278
SN - 1572-8862
ER -
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@article{2014_Gogoleva,
author = {Natalya Gogoleva and Ekaterina Zorina Tikhonova and Grigory Aleksandrov and Anatoly Lermontov and Nikolay Efimov and Artem Bogomyakov and Elena Ugolkova and Sergey Kolotilov and Aleksey Sidorov and Vadim Minin and Vladimir Novotortsev and Igor Eremenko},
title = {1,1-Cyclohexanediacetate as New Bridging Ligand for Assembling of Homo- and Heterometallic Molecular Complexes with Cu 3 II , Cu 2 II Ln 2 III (Ln = Sm or Gd) and Ni 2 II Gd 2 III Cores: Synthesis, Structure and Magnetic Properties},
journal = {Journal of Cluster Science},
year = {2014},
volume = {26},
publisher = {Springer Nature},
month = {jun},
url = {https://doi.org/10.1007/s10876-014-0740-2},
number = {1},
pages = {137--155},
doi = {10.1007/s10876-014-0740-2}
}
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MLA
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Gogoleva, Natalya, et al. “1,1-Cyclohexanediacetate as New Bridging Ligand for Assembling of Homo- and Heterometallic Molecular Complexes with Cu 3 II , Cu 2 II Ln 2 III (Ln = Sm or Gd) and Ni 2 II Gd 2 III Cores: Synthesis, Structure and Magnetic Properties.” Journal of Cluster Science, vol. 26, no. 1, Jun. 2014, pp. 137-155. https://doi.org/10.1007/s10876-014-0740-2.