Palladium-catalyzed activation of E-E and C-E bonds in diaryl dichalcogenides (E = S, Se) under microwave irradiation conditions
Publication type: Journal Article
Publication date: 2005-03-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
The first example of palladium-catalyzed stereoselective addition of diphenyl disulfide and diphenyl diselenide to the triple bond of terminal alkynes under microwave irradiation conditions is described. It was found that both the element—element (E-E) and carbon—element bonds can be activated in the catalytic system studied. The products of both reactions were isolated in quantitative yields. According to quantum-chemical calculations, the reaction mechanism involves the oxidative addition of the E-E bond to Pd0. Depending on the microwave power and reaction conditions, the next stage is either the reaction with alkyne or the carbon—element bond activation. The product of the oxidative addition of Ph2Se2 to Pd0, namely, dinuclear complex [Pd2(SePh)4(PPh3 2], was detected by 31P{1H}NMR spectroscopy directly in the Ph2Se2/PPh3 melt formed under microwave irradiation conditions.
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Ananikov V. P., Orlov N. V., Beletskaya I. P. Palladium-catalyzed activation of E-E and C-E bonds in diaryl dichalcogenides (E = S, Se) under microwave irradiation conditions // Russian Chemical Bulletin. 2005. Vol. 54. No. 3. pp. 576-587.
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Ananikov V. P., Orlov N. V., Beletskaya I. P. Palladium-catalyzed activation of E-E and C-E bonds in diaryl dichalcogenides (E = S, Se) under microwave irradiation conditions // Russian Chemical Bulletin. 2005. Vol. 54. No. 3. pp. 576-587.
Cite this
RIS
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TY - JOUR
DO - 10.1007/s11172-005-0292-6
UR - https://doi.org/10.1007/s11172-005-0292-6
TI - Palladium-catalyzed activation of E-E and C-E bonds in diaryl dichalcogenides (E = S, Se) under microwave irradiation conditions
T2 - Russian Chemical Bulletin
AU - Ananikov, V P
AU - Orlov, N V
AU - Beletskaya, I P
PY - 2005
DA - 2005/03/01
PB - Springer Nature
SP - 576-587
IS - 3
VL - 54
SN - 1066-5285
SN - 1573-9171
ER -
Cite this
BibTex (up to 50 authors)
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@article{2005_Ananikov,
author = {V P Ananikov and N V Orlov and I P Beletskaya},
title = {Palladium-catalyzed activation of E-E and C-E bonds in diaryl dichalcogenides (E = S, Se) under microwave irradiation conditions},
journal = {Russian Chemical Bulletin},
year = {2005},
volume = {54},
publisher = {Springer Nature},
month = {mar},
url = {https://doi.org/10.1007/s11172-005-0292-6},
number = {3},
pages = {576--587},
doi = {10.1007/s11172-005-0292-6}
}
Cite this
MLA
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Ananikov, V. P., et al. “Palladium-catalyzed activation of E-E and C-E bonds in diaryl dichalcogenides (E = S, Se) under microwave irradiation conditions.” Russian Chemical Bulletin, vol. 54, no. 3, Mar. 2005, pp. 576-587. https://doi.org/10.1007/s11172-005-0292-6.
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