Thermal decomposition of dinuclear complexes LM(μ-OOCR)4ML (L is α-substituted pyridine)
I.G. Fomina
1
,
Zh V Dobrokhotova
1
,
G.G. Aleksandrov
1
,
M. A. Kiskin
1
,
M. A. Bykov
2
,
V. N. Ikorskii
3
,
V. M. Novotortsev
1
,
Publication type: Journal Article
Publication date: 2007-09-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
The solid-state thermal decomposition of the dinuclear pivalate complexes LM(μ-OOCR)4ML, both those synthesized earlier (M = MnII, FeII, or CoII; L = 2,6-(NH2)2C5H3N)) and new complexes (M = CuII; L = 2,6-(NH2)2C5H3N or (2-NH2)(6-CH3)C5H3N), was studied by differential scanning calorimetry and thermogravimetry. The decomposition of the CoII complexes is accompanied by the aggregation to form the volatile octanuclear complex Co8(μ4-O)2(μn-OOCCMe3)12 (n = 2 or 3), whereas the thermolysis of the MnII, FeII, and CuII complexes is destructive, the phase composition of the decomposition products being substantially dependent on the nature of metal and the α substituent R in the apical organic ligand.
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Fomina I. et al. Thermal decomposition of dinuclear complexes LM(μ-OOCR)4ML (L is α-substituted pyridine) // Russian Chemical Bulletin. 2007. Vol. 56. No. 9. pp. 1722-1730.
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Fomina I., Dobrokhotova Z. V., Aleksandrov G., Kiskin M. A., Bykov M. A., Ikorskii V. N., Novotortsev V. M., Eremenko I. L. Thermal decomposition of dinuclear complexes LM(μ-OOCR)4ML (L is α-substituted pyridine) // Russian Chemical Bulletin. 2007. Vol. 56. No. 9. pp. 1722-1730.
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RIS
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TY - JOUR
DO - 10.1007/s11172-007-0267-x
UR - https://doi.org/10.1007/s11172-007-0267-x
TI - Thermal decomposition of dinuclear complexes LM(μ-OOCR)4ML (L is α-substituted pyridine)
T2 - Russian Chemical Bulletin
AU - Fomina, I.G.
AU - Dobrokhotova, Zh V
AU - Aleksandrov, G.G.
AU - Kiskin, M. A.
AU - Bykov, M. A.
AU - Ikorskii, V. N.
AU - Novotortsev, V. M.
AU - Eremenko, I. L.
PY - 2007
DA - 2007/09/01
PB - Springer Nature
SP - 1722-1730
IS - 9
VL - 56
SN - 1066-5285
SN - 1573-9171
ER -
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BibTex (up to 50 authors)
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@article{2007_Fomina,
author = {I.G. Fomina and Zh V Dobrokhotova and G.G. Aleksandrov and M. A. Kiskin and M. A. Bykov and V. N. Ikorskii and V. M. Novotortsev and I. L. Eremenko},
title = {Thermal decomposition of dinuclear complexes LM(μ-OOCR)4ML (L is α-substituted pyridine)},
journal = {Russian Chemical Bulletin},
year = {2007},
volume = {56},
publisher = {Springer Nature},
month = {sep},
url = {https://doi.org/10.1007/s11172-007-0267-x},
number = {9},
pages = {1722--1730},
doi = {10.1007/s11172-007-0267-x}
}
Cite this
MLA
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Fomina, I.G., et al. “Thermal decomposition of dinuclear complexes LM(μ-OOCR)4ML (L is α-substituted pyridine).” Russian Chemical Bulletin, vol. 56, no. 9, Sep. 2007, pp. 1722-1730. https://doi.org/10.1007/s11172-007-0267-x.