Russian Chemical Bulletin

, volume 56 , issue 12 , pages 2448-2455

Polyalkoxybenzenes from plant raw materials 1. Isolation of polyalkoxybenzenes from CO2 extracts of Umbelliferae plant seeds

V. V. Semenov ¹

V V Rusak ¹

E M Chartov ¹

M I Zaretskii ¹

L D Konyushkin ¹

S I Firgang ¹

A. O. Chizhov ¹

V V Elkin ¹

N N Latin ²

V M Bonashek ²

O N Staseva ²

Hide authors affiliations Show authors affiliations: 2 affiliations

N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation |

OJSC Karavan Belozernyi, Krasnodar, Russian Federation |

Publication type: Journal Article

Publication date: 2007-12-01

Springer Nature

Russian Chemical Bulletin

scimago Q3

SJR: 0.305

CiteScore: 2.8

Impact factor: —

ISSN: 10665285, 15739171

DOI: 10.1007/s11172-007-0389-1

Copy DOI

General Chemistry

Abstract

For the search for a domestic natural source of allylpolyalkoxybenzenes and development of an effective process for their isolation, CO2 extracts of several varieties of parsley, dill, celery, caraway, and nutmeg were analyzed systematically for the first time by GC/MS and GLC techniques. The varieties with high contents of myristicin, elemicin, allyltetramethoxybenzene, apiol, and dillapiol were identified. The conditions of CO2 extraction for obtaining concentrates with minimum contents of the distillation residues were selected. Using high performance fractional distillation, polyalkoxyallylbenzenes with 98–99% purity were isolated from the concentrates on a pilot unit. By isomerization of some allylbenzenes followed by ozonolysis under specially selected conditions, apiol-and dillapiolaldehydes were obtained in 75–80% yields.

Found

2 citations

Nasyrova Darina

🤝

23 publications, 91 citations

h-index: 5

N.D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences

Research interests

Crystallography

X-ray diffraction (XRD)

X-ray diffraction analysis

1 citation

Khrustalev Victor

DSc in Chemistry, professor, professor of the Russian Academy of Sciences

327 publications, 4 137 citations, 4 reviews

h-index: 30

N.D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences

Peoples' Friendship University of Russia

1 citation

Komogortsev Andrey

🥼 🤝

PhD in Chemistry

106 publications, 769 citations, 3 reviews

h-index: 15

N.D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences

Research interests

Photochemistry

1 citation

Borisov Roman

🤝

PhD in Chemistry

184 publications, 1 731 citations, 20 reviews

h-index: 21

A.V. Topchiev Institute of Petrochemical Synthesis RAS

Peoples' Friendship University of Russia

Research interests

Mass Spectrometry

1 citation

Volcho Konstantin

DSc in Chemistry, professor of the Russian Academy of Sciences

280 publications, 3 941 citations, 67 reviews

h-index: 32

N.N. Vorozhtsov Novosibirsk Institute of Organic Chemistry of the Siberian Branch of the Russian Academy of Sciences

1 citation

Shevchenko Oksana

🤝

PhD in Biological/biomedical sciences

106 publications, 1 179 citations

h-index: 18

Institute of Chemistry Komi SC of the Ural Branch of the Russian Academy of Sciences

Research interests

Antioxidants

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GOST Copy

Semenov V. V. et al. Polyalkoxybenzenes from plant raw materials 1. Isolation of polyalkoxybenzenes from CO2 extracts of Umbelliferae plant seeds // Russian Chemical Bulletin. 2007. Vol. 56. No. 12. pp. 2448-2455.

GOST all authors (up to 50) Copy

Semenov V. V., Rusak V. V., Chartov E. M., Zaretskii M. I., Konyushkin L. D., Firgang S. I., Chizhov A. O., Elkin V. V., Latin N. N., Bonashek V. M., Staseva O. N. Polyalkoxybenzenes from plant raw materials 1. Isolation of polyalkoxybenzenes from CO2 extracts of Umbelliferae plant seeds // Russian Chemical Bulletin. 2007. Vol. 56. No. 12. pp. 2448-2455.

RIS |

Cite this

RIS Copy

TY - JOUR

DO - 10.1007/s11172-007-0389-1

UR - https://doi.org/10.1007/s11172-007-0389-1

TI - Polyalkoxybenzenes from plant raw materials 1. Isolation of polyalkoxybenzenes from CO2 extracts of Umbelliferae plant seeds

T2 - Russian Chemical Bulletin

AU - Semenov, V. V.

AU - Rusak, V V

AU - Chartov, E M

AU - Zaretskii, M I

AU - Konyushkin, L D

AU - Firgang, S I

AU - Chizhov, A. O.

AU - Elkin, V V

AU - Latin, N N

AU - Bonashek, V M

AU - Staseva, O N

PY - 2007

DA - 2007/12/01

PB - Springer Nature

SP - 2448-2455

IS - 12

VL - 56

SN - 1066-5285

SN - 1573-9171

ER -

BibTex |

Cite this

BibTex (up to 50 authors) Copy

@article{2007_Semenov,

author = {V. V. Semenov and V V Rusak and E M Chartov and M I Zaretskii and L D Konyushkin and S I Firgang and A. O. Chizhov and V V Elkin and N N Latin and V M Bonashek and O N Staseva},

title = {Polyalkoxybenzenes from plant raw materials 1. Isolation of polyalkoxybenzenes from CO2 extracts of Umbelliferae plant seeds},

journal = {Russian Chemical Bulletin},

year = {2007},

volume = {56},

publisher = {Springer Nature},

month = {dec},

url = {https://doi.org/10.1007/s11172-007-0389-1},

number = {12},

pages = {2448--2455},

doi = {10.1007/s11172-007-0389-1}

}

MLA

Cite this

MLA Copy

Semenov, V. V., et al. “Polyalkoxybenzenes from plant raw materials 1. Isolation of polyalkoxybenzenes from CO2 extracts of Umbelliferae plant seeds.” Russian Chemical Bulletin, vol. 56, no. 12, Dec. 2007, pp. 2448-2455. https://doi.org/10.1007/s11172-007-0389-1.

Publisher

Springer Nature

Journal

Russian Chemical Bulletin

scimago Q3

SJR

0.305

CiteScore

2.8

Impact factor

—

ISSN

10665285 (Print)

15739171 (Electronic)