Pivalates with the MII 4O4 cubane core (M = Co, Ni): synthesis, structure, magnetic properties, and solid-state thermolysis
I.G. Fomina
1
,
Zh V Dobrokhotova
1
,
G.G. Aleksandrov
1
,
O Yu Proshenkina
1
,
M.L. Kovba
2
,
A S Bogomyakov
3
,
V. N. Ikorskii
3
,
V. M. Novotortsev
1
,
Publication type: Journal Article
Publication date: 2009-01-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
Methods were developed for the controlled thermal synthesis of high-spin cubane-like pivalates {MII 4(μ3−OR)4} (M = Co or Ni; R = H or Me) starting from mono-and polynuclear complexes. The solid-state thermal decomposition of the known pivalate clusters [MII 4(μ3−OMe)4−(μ2−OOCBut)2(η2−OOCBut)2(MeOH)4] and the new clusters [M 4 II (μ3)−OH4(η1−OOCBut)3−(μ−(NH2)2C6H2Me2)3(η1−(NH2)2C6H2Me2)3]+(OOCBut)− (M = Co or Ni) was studied by differential scanning calorimetry and thermogravimetry. The thermolysis of cubane-like CoII and NiII pivalates is a destructive process. The phase composition of the decomposition products is determined by the nature of coordinated ligands and the structural features of the metal core.
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Fomina I. et al. Pivalates with the MII 4O4 cubane core (M = Co, Ni): synthesis, structure, magnetic properties, and solid-state thermolysis // Russian Chemical Bulletin. 2009. Vol. 58. No. 1. pp. 11-20.
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Fomina I., Dobrokhotova Z. V., Aleksandrov G., Proshenkina O. Yu., Kovba M., Bogomyakov A. S., Ikorskii V. N., Novotortsev V. M., Eremenko I. L. Pivalates with the MII 4O4 cubane core (M = Co, Ni): synthesis, structure, magnetic properties, and solid-state thermolysis // Russian Chemical Bulletin. 2009. Vol. 58. No. 1. pp. 11-20.
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TY - JOUR
DO - 10.1007/s11172-009-0002-x
UR - https://doi.org/10.1007/s11172-009-0002-x
TI - Pivalates with the MII 4O4 cubane core (M = Co, Ni): synthesis, structure, magnetic properties, and solid-state thermolysis
T2 - Russian Chemical Bulletin
AU - Fomina, I.G.
AU - Dobrokhotova, Zh V
AU - Aleksandrov, G.G.
AU - Proshenkina, O Yu
AU - Kovba, M.L.
AU - Bogomyakov, A S
AU - Ikorskii, V. N.
AU - Novotortsev, V. M.
AU - Eremenko, I. L.
PY - 2009
DA - 2009/01/01
PB - Springer Nature
SP - 11-20
IS - 1
VL - 58
SN - 1066-5285
SN - 1573-9171
ER -
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BibTex (up to 50 authors)
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@article{2009_Fomina,
author = {I.G. Fomina and Zh V Dobrokhotova and G.G. Aleksandrov and O Yu Proshenkina and M.L. Kovba and A S Bogomyakov and V. N. Ikorskii and V. M. Novotortsev and I. L. Eremenko},
title = {Pivalates with the MII 4O4 cubane core (M = Co, Ni): synthesis, structure, magnetic properties, and solid-state thermolysis},
journal = {Russian Chemical Bulletin},
year = {2009},
volume = {58},
publisher = {Springer Nature},
month = {jan},
url = {https://doi.org/10.1007/s11172-009-0002-x},
number = {1},
pages = {11--20},
doi = {10.1007/s11172-009-0002-x}
}
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MLA
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Fomina, I.G., et al. “Pivalates with the MII 4O4 cubane core (M = Co, Ni): synthesis, structure, magnetic properties, and solid-state thermolysis.” Russian Chemical Bulletin, vol. 58, no. 1, Jan. 2009, pp. 11-20. https://doi.org/10.1007/s11172-009-0002-x.