Synthesis and nitration of N,Ń-bis(3-R-furoxan-4-yl) methylenediamines
A O Finogenov
1
,
M A Epishina
1
,
A.S Kulikov
1
,
N N Makhova
1
,
I V Ananev
2
,
V.A. Tartakovsky
1
Publication type: Journal Article
Publication date: 2010-11-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
A Mannich reaction of 4-amino-3-R-furoxans with paraformaldehyde in 10% aqueous H2SO4 led to the high yields of N,N′-bis(3-R-furoxan-4-yl)methylenediamines, whose structure (using R = Me as an example) was confirmed by X-ray diffraction study. The N,N′-bis-(3-R-furoxan-4-yl)methylenediamines obtained were nitrated to N,N′-dinitro-N,N′-bis-(3-R-furoxan-4-yl)methylenediamines upon the action of 100% HNO3 in acetic or trifluoroacetic anhydride.
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11
Total citations:
11
Citations from 2024:
1
(9.09%)
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GOST
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Finogenov A. O. et al. Synthesis and nitration of N,Ń-bis(3-R-furoxan-4-yl) methylenediamines // Russian Chemical Bulletin. 2010. Vol. 59. No. 11. pp. 2108-2113.
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Finogenov A. O., Epishina M. A., Kulikov A., Makhova N. N., Ananev I. V., Tartakovsky V. Synthesis and nitration of N,Ń-bis(3-R-furoxan-4-yl) methylenediamines // Russian Chemical Bulletin. 2010. Vol. 59. No. 11. pp. 2108-2113.
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RIS
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TY - JOUR
DO - 10.1007/s11172-010-0363-1
UR - https://doi.org/10.1007/s11172-010-0363-1
TI - Synthesis and nitration of N,Ń-bis(3-R-furoxan-4-yl) methylenediamines
T2 - Russian Chemical Bulletin
AU - Finogenov, A O
AU - Epishina, M A
AU - Kulikov, A.S
AU - Makhova, N N
AU - Ananev, I V
AU - Tartakovsky, V.A.
PY - 2010
DA - 2010/11/01
PB - Springer Nature
SP - 2108-2113
IS - 11
VL - 59
SN - 1066-5285
SN - 1573-9171
ER -
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BibTex (up to 50 authors)
Copy
@article{2010_Finogenov,
author = {A O Finogenov and M A Epishina and A.S Kulikov and N N Makhova and I V Ananev and V.A. Tartakovsky},
title = {Synthesis and nitration of N,Ń-bis(3-R-furoxan-4-yl) methylenediamines},
journal = {Russian Chemical Bulletin},
year = {2010},
volume = {59},
publisher = {Springer Nature},
month = {nov},
url = {https://doi.org/10.1007/s11172-010-0363-1},
number = {11},
pages = {2108--2113},
doi = {10.1007/s11172-010-0363-1}
}
Cite this
MLA
Copy
Finogenov, A. O., et al. “Synthesis and nitration of N,Ń-bis(3-R-furoxan-4-yl) methylenediamines.” Russian Chemical Bulletin, vol. 59, no. 11, Nov. 2010, pp. 2108-2113. https://doi.org/10.1007/s11172-010-0363-1.