A study of the reaction mechanism of 3-nitro-4-R-furoxans formation by nitrosation of dipotassium salts of 1-hydroxyimino-2,2-dinitro-1-R-ethanes
Тип публикации: Journal Article
Дата публикации: 2011-05-01
scimago Q3
БС2
SJR: 0.305
CiteScore: 2.8
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ISSN: 10665285, 15739171
General Chemistry
Краткое описание
The mechanism proposed earlier for explanation of the furoxan ring formation in the nitrosation of dipotassium salts of 1-hydroxyimino-2,2-dinitro-1-R-ethanes with NaNO2/AcOH was confirmed experimentally by determining the ionization constants of the dinitromethyl and oxime fragments in the starting dipotassium salt and by examining 1H, 13C, 14N, and 15N NMR and mass spectra of isomeric 3(4)-nitro-4(3)-R-furoxans with the 15N(5) and 15N(2) ring atoms, respectively, and 3,4-diarylfuroxan with both 15N-labeled ring atoms. A comparative analysis of the IR and Raman spectra of the 15N-labeled furoxan derivatives obtained and their unlabeled analogs allowed refinement of the literature data on interpretation of the vibrational spectra of furoxan derivatives.
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Ovchinnikov I. V. et al. A study of the reaction mechanism of 3-nitro-4-R-furoxans formation by nitrosation of dipotassium salts of 1-hydroxyimino-2,2-dinitro-1-R-ethanes // Russian Chemical Bulletin. 2011. Vol. 60. No. 5. pp. 855-860.
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Ovchinnikov I. V., Strelenko Y., Popov N. A., Finogenov A. O., Makhova N. N. A study of the reaction mechanism of 3-nitro-4-R-furoxans formation by nitrosation of dipotassium salts of 1-hydroxyimino-2,2-dinitro-1-R-ethanes // Russian Chemical Bulletin. 2011. Vol. 60. No. 5. pp. 855-860.
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TY - JOUR
DO - 10.1007/s11172-011-0134-7
UR - https://doi.org/10.1007/s11172-011-0134-7
TI - A study of the reaction mechanism of 3-nitro-4-R-furoxans formation by nitrosation of dipotassium salts of 1-hydroxyimino-2,2-dinitro-1-R-ethanes
T2 - Russian Chemical Bulletin
AU - Ovchinnikov, I V
AU - Strelenko, Yu.A.
AU - Popov, N. A.
AU - Finogenov, A O
AU - Makhova, N N
PY - 2011
DA - 2011/05/01
PB - Springer Nature
SP - 855-860
IS - 5
VL - 60
SN - 1066-5285
SN - 1573-9171
ER -
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@article{2011_Ovchinnikov,
author = {I V Ovchinnikov and Yu.A. Strelenko and N. A. Popov and A O Finogenov and N N Makhova},
title = {A study of the reaction mechanism of 3-nitro-4-R-furoxans formation by nitrosation of dipotassium salts of 1-hydroxyimino-2,2-dinitro-1-R-ethanes},
journal = {Russian Chemical Bulletin},
year = {2011},
volume = {60},
publisher = {Springer Nature},
month = {may},
url = {https://doi.org/10.1007/s11172-011-0134-7},
number = {5},
pages = {855--860},
doi = {10.1007/s11172-011-0134-7}
}
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Ovchinnikov, I. V., et al. “A study of the reaction mechanism of 3-nitro-4-R-furoxans formation by nitrosation of dipotassium salts of 1-hydroxyimino-2,2-dinitro-1-R-ethanes.” Russian Chemical Bulletin, vol. 60, no. 5, May. 2011, pp. 855-860. https://doi.org/10.1007/s11172-011-0134-7.
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