Synthesis, structure, electrochemical and magnetic properties of 2,6-bis(5-trifluoromethylpyrazol-3-yl)pyridine and its NiII complexes
E F Khmara
1
,
D.L. Chizhov
1
,
A. A. Sidorov
2
,
G.G. Aleksandrov
2
,
P A Slepukhin
1
,
M. A. Kiskin
2
,
K L Tokarev
2
,
V I Filyakova
1
,
G.L. Rusinov
1
,
I V Smolyaninov
3
,
A S Bogomyakov
4
,
D V Starichenko
5
,
Yu.N. Shvachko
5
,
A. V. Korolev
5
,
I. L. Eremenko
2
,
V. N. Charushin
1
Тип публикации: Journal Article
Дата публикации: 2012-02-01
scimago Q3
БС2
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Краткое описание
Abstract2,6-Bis(5-trifluoromethylpyrazol-3-yl)pyridine (H2L) and its mono-, tri-, and tetranuclear NiII complexes were synthesized for the first time. All the obtained compounds were characterized by single-crystal X-ray diffraction analysis. In the complexes, 2,6-bis(5-trifluoromethylpyrazol-3-yl)pyridine exists in the neutral and dianionic forms and exhibits different coordination modes (κ3-, μ2-κ3:κ1-, and μ3-κ3:κ1:κ1). The electrochemical and magnetic properties of all compounds were studied. The tetranuclear NiII complex with the L2− dianion is reduced in two sequential reversible one-electron steps.
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Khmara E. F. et al. Synthesis, structure, electrochemical and magnetic properties of 2,6-bis(5-trifluoromethylpyrazol-3-yl)pyridine and its NiII complexes // Russian Chemical Bulletin. 2012. Vol. 61. No. 2. pp. 313-325.
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Khmara E. F., Chizhov D., Sidorov A. A., Aleksandrov G., Slepukhin P. A., Kiskin M. A., Tokarev K. L., Filyakova V. I., Rusinov G., Smolyaninov I. V., Bogomyakov A. S., Starichenko D. V., Shvachko Y., Korolev A. V., Eremenko I. L., Charushin V. N. Synthesis, structure, electrochemical and magnetic properties of 2,6-bis(5-trifluoromethylpyrazol-3-yl)pyridine and its NiII complexes // Russian Chemical Bulletin. 2012. Vol. 61. No. 2. pp. 313-325.
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TY - JOUR
DO - 10.1007/s11172-012-0044-3
UR - https://doi.org/10.1007/s11172-012-0044-3
TI - Synthesis, structure, electrochemical and magnetic properties of 2,6-bis(5-trifluoromethylpyrazol-3-yl)pyridine and its NiII complexes
T2 - Russian Chemical Bulletin
AU - Khmara, E F
AU - Chizhov, D.L.
AU - Sidorov, A. A.
AU - Aleksandrov, G.G.
AU - Slepukhin, P A
AU - Kiskin, M. A.
AU - Tokarev, K L
AU - Filyakova, V I
AU - Rusinov, G.L.
AU - Smolyaninov, I V
AU - Bogomyakov, A S
AU - Starichenko, D V
AU - Shvachko, Yu.N.
AU - Korolev, A. V.
AU - Eremenko, I. L.
AU - Charushin, V. N.
PY - 2012
DA - 2012/02/01
PB - Springer Nature
SP - 313-325
IS - 2
VL - 61
SN - 1066-5285
SN - 1573-9171
ER -
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@article{2012_Khmara,
author = {E F Khmara and D.L. Chizhov and A. A. Sidorov and G.G. Aleksandrov and P A Slepukhin and M. A. Kiskin and K L Tokarev and V I Filyakova and G.L. Rusinov and I V Smolyaninov and A S Bogomyakov and D V Starichenko and Yu.N. Shvachko and A. V. Korolev and I. L. Eremenko and V. N. Charushin},
title = {Synthesis, structure, electrochemical and magnetic properties of 2,6-bis(5-trifluoromethylpyrazol-3-yl)pyridine and its NiII complexes},
journal = {Russian Chemical Bulletin},
year = {2012},
volume = {61},
publisher = {Springer Nature},
month = {feb},
url = {https://doi.org/10.1007/s11172-012-0044-3},
number = {2},
pages = {313--325},
doi = {10.1007/s11172-012-0044-3}
}
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Khmara, E. F., et al. “Synthesis, structure, electrochemical and magnetic properties of 2,6-bis(5-trifluoromethylpyrazol-3-yl)pyridine and its NiII complexes.” Russian Chemical Bulletin, vol. 61, no. 2, Feb. 2012, pp. 313-325. https://doi.org/10.1007/s11172-012-0044-3.