Structure determination of bis(4Z)-1-(2-azidoethyl)-4-[(pyridin-2-yl) methylidene]-2-thiolatoimidazol-5(4H)-onedicopper chloride from X-ray powder diffraction data
A.V. Mironov
1
,
E. V. ANTIPOV
1
,
E K Beloglazkina
1
,
A G Majouga
1
,
O O Krasnovskaya
1
,
V M Gerasimov
1
,
N. V. Zyk
1
Publication type: Journal Article
Publication date: 2013-03-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
The new tridentate organic N2S-type ligand, (4Z)-1-(2-azidoethyl)-4-[(pyridin-2-yl)-methylidene]-2-thioxoimidazol-5(4H)-one (LH), was synthesized. The reaction of LH with copper(II) chloride in a CH2Cl2/MeOH mixture afforded the coordination compound of the composition L2Cu2Cl (3). The crystal structure of 3 was solved and refined from X-ray powder diffraction data. Complex 3 has a binuclear structure with a short interatomic Cu-Cu distance and one bridging chlorine atom, which is located almost symmetrically with respect to both metal atoms. The planar organic ligands are noncoplanar and are at an angle of 53.56(1)° to each other.
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Mironov A. et al. Structure determination of bis(4Z)-1-(2-azidoethyl)-4-[(pyridin-2-yl) methylidene]-2-thiolatoimidazol-5(4H)-onedicopper chloride from X-ray powder diffraction data // Russian Chemical Bulletin. 2013. Vol. 62. No. 3. pp. 672-677.
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Mironov A., ANTIPOV E. V., Beloglazkina E. K., Majouga A. G., Krasnovskaya O. O., Gerasimov V. M., Zyk N. V. Structure determination of bis(4Z)-1-(2-azidoethyl)-4-[(pyridin-2-yl) methylidene]-2-thiolatoimidazol-5(4H)-onedicopper chloride from X-ray powder diffraction data // Russian Chemical Bulletin. 2013. Vol. 62. No. 3. pp. 672-677.
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TY - JOUR
DO - 10.1007/s11172-013-0090-5
UR - http://link.springer.com/10.1007/s11172-013-0090-5
TI - Structure determination of bis(4Z)-1-(2-azidoethyl)-4-[(pyridin-2-yl) methylidene]-2-thiolatoimidazol-5(4H)-onedicopper chloride from X-ray powder diffraction data
T2 - Russian Chemical Bulletin
AU - Mironov, A.V.
AU - ANTIPOV, E. V.
AU - Beloglazkina, E K
AU - Majouga, A G
AU - Krasnovskaya, O O
AU - Gerasimov, V M
AU - Zyk, N. V.
PY - 2013
DA - 2013/03/01
PB - Springer Nature
SP - 672-677
IS - 3
VL - 62
SN - 1066-5285
SN - 1573-9171
ER -
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BibTex (up to 50 authors)
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@article{2013_Mironov,
author = {A.V. Mironov and E. V. ANTIPOV and E K Beloglazkina and A G Majouga and O O Krasnovskaya and V M Gerasimov and N. V. Zyk},
title = {Structure determination of bis(4Z)-1-(2-azidoethyl)-4-[(pyridin-2-yl) methylidene]-2-thiolatoimidazol-5(4H)-onedicopper chloride from X-ray powder diffraction data},
journal = {Russian Chemical Bulletin},
year = {2013},
volume = {62},
publisher = {Springer Nature},
month = {mar},
url = {http://link.springer.com/10.1007/s11172-013-0090-5},
number = {3},
pages = {672--677},
doi = {10.1007/s11172-013-0090-5}
}
Cite this
MLA
Copy
Mironov, A.V., et al. “Structure determination of bis(4Z)-1-(2-azidoethyl)-4-[(pyridin-2-yl) methylidene]-2-thiolatoimidazol-5(4H)-onedicopper chloride from X-ray powder diffraction data.” Russian Chemical Bulletin, vol. 62, no. 3, Mar. 2013, pp. 672-677. http://link.springer.com/10.1007/s11172-013-0090-5.