Synthesis, structure, and ESR spectra of the new heteronuclear complex {Li4(VO)2[(OOC)2C(H)Bu]4(H2O)8}·H2O
E S Bazhina
1
,
G.G. Aleksandrov
1
,
N. N. Efimov
1
,
E. A. Ugolkova
1
,
V V Minin
1
,
A. A. Sidorov
1
,
V. M. Novotortsev
1
,
Publication type: Journal Article
Publication date: 2013-04-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
The reaction of an aqueous solution of vanadyl sulfate VOSO4·3H2O, butylmalonic acid (H2Bumal = C4H10(COOH)2), and lithium carbonate at pH ∼4–5 gave crystals of the complex Li4(VO)2(Bumal)4(H2O)8]·H2O (1). The structure of complex 1 was established by X-ray diffraction analysis. The molecule of complex 1 consists of two mononuclear bischelate dianionic units {VO(Bumal)2(H2O)} linked by four lithium ions to form the hexanuclear heterometallic {V2Li4} structure. The crystals and an ethanolic solution of compound 1 were studied by ESR spectroscopy.
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Bazhina E. S. et al. Synthesis, structure, and ESR spectra of the new heteronuclear complex {Li4(VO)2[(OOC)2C(H)Bu]4(H2O)8}·H2O // Russian Chemical Bulletin. 2013. Vol. 62. No. 4. pp. 962-965.
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Bazhina E. S., Aleksandrov G., Efimov N. N., Ugolkova E. A., Minin V. V., Sidorov A. A., Novotortsev V. M., Eremenko I. L. Synthesis, structure, and ESR spectra of the new heteronuclear complex {Li4(VO)2[(OOC)2C(H)Bu]4(H2O)8}·H2O // Russian Chemical Bulletin. 2013. Vol. 62. No. 4. pp. 962-965.
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RIS
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TY - JOUR
DO - 10.1007/s11172-013-0125-y
UR - https://doi.org/10.1007/s11172-013-0125-y
TI - Synthesis, structure, and ESR spectra of the new heteronuclear complex {Li4(VO)2[(OOC)2C(H)Bu]4(H2O)8}·H2O
T2 - Russian Chemical Bulletin
AU - Bazhina, E S
AU - Aleksandrov, G.G.
AU - Efimov, N. N.
AU - Ugolkova, E. A.
AU - Minin, V V
AU - Sidorov, A. A.
AU - Novotortsev, V. M.
AU - Eremenko, I. L.
PY - 2013
DA - 2013/04/01
PB - Springer Nature
SP - 962-965
IS - 4
VL - 62
SN - 1066-5285
SN - 1573-9171
ER -
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BibTex (up to 50 authors)
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@article{2013_Bazhina,
author = {E S Bazhina and G.G. Aleksandrov and N. N. Efimov and E. A. Ugolkova and V V Minin and A. A. Sidorov and V. M. Novotortsev and I. L. Eremenko},
title = {Synthesis, structure, and ESR spectra of the new heteronuclear complex {Li4(VO)2[(OOC)2C(H)Bu]4(H2O)8}·H2O},
journal = {Russian Chemical Bulletin},
year = {2013},
volume = {62},
publisher = {Springer Nature},
month = {apr},
url = {https://doi.org/10.1007/s11172-013-0125-y},
number = {4},
pages = {962--965},
doi = {10.1007/s11172-013-0125-y}
}
Cite this
MLA
Copy
Bazhina, E. S., et al. “Synthesis, structure, and ESR spectra of the new heteronuclear complex {Li4(VO)2[(OOC)2C(H)Bu]4(H2O)8}·H2O.” Russian Chemical Bulletin, vol. 62, no. 4, Apr. 2013, pp. 962-965. https://doi.org/10.1007/s11172-013-0125-y.