Ammonolysis of boron-substituted chlorosilylmethyl ortho-carborane derivatives
Publication type: Journal Article
Publication date: 2014-10-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
We studied the ammonolysis of boron-substituted chlorosilylmethyl ortho-carborane derivatives and co-ammonolysis with trimethylchlorosilane. The reaction affords carboranylmethyl(organo)silanes with terminal aminosilane or trimethylsilyl groups. During ammonolysis, the bulky carboranylmethyl groups hinder the intermolecular condensation of intermediate products with aminosilane groups and favors the formation of low-molecular-weight organosilazanes not only from mono- and dichlorosilanes, but also from carboranylmethyltrichlorosilane. The Ccarborane-H groups having the acidic nature were found to be possibly involved in the formation of oligo(carboranylmethyl)silsesquiazane structure and its room-temperature structuring products.
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Izmailov B. A. et al. Ammonolysis of boron-substituted chlorosilylmethyl ortho-carborane derivatives // Russian Chemical Bulletin. 2014. Vol. 63. No. 10. pp. 2338-2342.
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Izmailov B. A., Qi S., Markova G. D., Vasnev V. A. Ammonolysis of boron-substituted chlorosilylmethyl ortho-carborane derivatives // Russian Chemical Bulletin. 2014. Vol. 63. No. 10. pp. 2338-2342.
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TY - JOUR
DO - 10.1007/s11172-014-0744-y
UR - https://doi.org/10.1007/s11172-014-0744-y
TI - Ammonolysis of boron-substituted chlorosilylmethyl ortho-carborane derivatives
T2 - Russian Chemical Bulletin
AU - Izmailov, B A
AU - Qi, Shisheng
AU - Markova, G. D.
AU - Vasnev, V. A.
PY - 2014
DA - 2014/10/01
PB - Springer Nature
SP - 2338-2342
IS - 10
VL - 63
SN - 1066-5285
SN - 1573-9171
ER -
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@article{2014_Izmailov,
author = {B A Izmailov and Shisheng Qi and G. D. Markova and V. A. Vasnev},
title = {Ammonolysis of boron-substituted chlorosilylmethyl ortho-carborane derivatives},
journal = {Russian Chemical Bulletin},
year = {2014},
volume = {63},
publisher = {Springer Nature},
month = {oct},
url = {https://doi.org/10.1007/s11172-014-0744-y},
number = {10},
pages = {2338--2342},
doi = {10.1007/s11172-014-0744-y}
}
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MLA
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Izmailov, B. A., et al. “Ammonolysis of boron-substituted chlorosilylmethyl ortho-carborane derivatives.” Russian Chemical Bulletin, vol. 63, no. 10, Oct. 2014, pp. 2338-2342. https://doi.org/10.1007/s11172-014-0744-y.