Springer Nature
Russian Chemical Bulletin
,  том 63 ,  издание 12 ,  страницы 2641-2646

Electrochemical C-H phosphorylation of 2-phenylpyridine in the presence of palladium salts

Тип публикации: Journal Article
Дата публикации: 2014-12-01
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ISSN: 10665285, 15739171
General Chemistry
Краткое описание
A new approach was developed to the introduction of the phosphonate group into arylpyridines using 2-phenylpyridine as an example. The approach is the electrochemical oxidation of a mixture of 2-phenylpyridine, diethyl phosphite, and palladium acetate at room temperature. An intermediate dipalladium cyclic complex was isolated that is formed by the ortho-palladation of 2-phenylpyridine and substitution of acetate ions by phosphonate ions. The preparative oxidation of this complex selectively results in the product of the phosphorylation of the C-H bond in 2-phenylpyridine.
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Dudkina Yu. B. et al. Electrochemical C-H phosphorylation of 2-phenylpyridine in the presence of palladium salts // Russian Chemical Bulletin. 2014. Vol. 63. No. 12. pp. 2641-2646.
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Dudkina Yu. B., Gryaznova T. V., Kataeva O. N., Budnikova Yu. H., Sinyashin O. G. Electrochemical C-H phosphorylation of 2-phenylpyridine in the presence of palladium salts // Russian Chemical Bulletin. 2014. Vol. 63. No. 12. pp. 2641-2646.
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TY - JOUR
DO - 10.1007/s11172-014-0792-3
UR - https://doi.org/10.1007/s11172-014-0792-3
TI - Electrochemical C-H phosphorylation of 2-phenylpyridine in the presence of palladium salts
T2 - Russian Chemical Bulletin
AU - Dudkina, Yu B
AU - Gryaznova, T V
AU - Kataeva, O. N.
AU - Budnikova, Yu H
AU - Sinyashin, O G
PY - 2014
DA - 2014/12/01
PB - Springer Nature
SP - 2641-2646
IS - 12
VL - 63
SN - 1066-5285
SN - 1573-9171
ER -
BibTex |
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@article{2014_Dudkina,
author = {Yu B Dudkina and T V Gryaznova and O. N. Kataeva and Yu H Budnikova and O G Sinyashin},
title = {Electrochemical C-H phosphorylation of 2-phenylpyridine in the presence of palladium salts},
journal = {Russian Chemical Bulletin},
year = {2014},
volume = {63},
publisher = {Springer Nature},
month = {dec},
url = {https://doi.org/10.1007/s11172-014-0792-3},
number = {12},
pages = {2641--2646},
doi = {10.1007/s11172-014-0792-3}
}
MLA
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Dudkina, Yu. B., et al. “Electrochemical C-H phosphorylation of 2-phenylpyridine in the presence of palladium salts.” Russian Chemical Bulletin, vol. 63, no. 12, Dec. 2014, pp. 2641-2646. https://doi.org/10.1007/s11172-014-0792-3.
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