Solid-phase syntheses of N-substituted carbamates. Reaction monitoring by gel-phase 13C NMR using a 13C enriched BAL-linker
Dolors Fernández-Forner
1
,
Josep M Huerta
1
,
Manel Ferrer
1
,
Gaspar Casals
1
,
Hamish Ryder
1
,
E. Giralt
2
,
Fernando Albericio
2
1
Research Center, Almirall Prodesfarma, Cardener 68-74, E-08024 Barcelona, Spain
|
Publication type: Journal Article
Publication date: 2002-05-01
scimago Q3
wos Q3
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
The solid-phase synthesis of N -substituted carbamates using the tris(alkoxy)benzyl (BAL) resin is reported. The incorporation of the primary amine was carried out by reductive amination, which was followed by reaction with an alkyl succinimidyl carbonate prepared in situ from the alcohol and N,N ′-disuccinimidyl carbonate (DSC). Final cleavage with trifluoroacetic acid rendered the target compounds. Scope and limitations of these methods are discussed. The reactions were controlled by gel-phase 13 C NMR using a 13 C enriched BAL resin.
Found
Nothing found, try to update filter.
Found
Nothing found, try to update filter.
Top-30
Journals
|
1
2
3
4
|
|
|
Journal of Combinatorial Chemistry
4 publications, 28.57%
|
|
|
Tetrahedron Letters
2 publications, 14.29%
|
|
|
Journal of Organic Chemistry
1 publication, 7.14%
|
|
|
Molecules
1 publication, 7.14%
|
|
|
Bulletin of the Korean Chemical Society
1 publication, 7.14%
|
|
|
Bioorganic and Medicinal Chemistry Letters
1 publication, 7.14%
|
|
|
Applied Catalysis A: General
1 publication, 7.14%
|
|
|
QSAR & Combinatorial Science
1 publication, 7.14%
|
|
|
Journal of Chemical Information and Modeling
1 publication, 7.14%
|
|
|
Chemical Reviews
1 publication, 7.14%
|
|
|
1
2
3
4
|
Publishers
|
1
2
3
4
5
6
7
|
|
|
American Chemical Society (ACS)
7 publications, 50%
|
|
|
Elsevier
4 publications, 28.57%
|
|
|
Wiley
2 publications, 14.29%
|
|
|
MDPI
1 publication, 7.14%
|
|
|
1
2
3
4
5
6
7
|
- We do not take into account publications without a DOI.
- Statistics recalculated weekly.
Are you a researcher?
Create a profile to get free access to personal recommendations for colleagues and new articles.
Metrics
14
Total citations:
14
Citations from 2024:
0
Cite this
GOST |
RIS |
BibTex |
MLA
Cite this
GOST
Copy
Fernández-Forner D. et al. Solid-phase syntheses of N-substituted carbamates. Reaction monitoring by gel-phase 13C NMR using a 13C enriched BAL-linker // Tetrahedron Letters. 2002. Vol. 43. No. 19. pp. 3543-3546.
GOST all authors (up to 50)
Copy
Fernández-Forner D., Huerta J. M., Ferrer M., Casals G., Ryder H., Giralt E., Albericio F. Solid-phase syntheses of N-substituted carbamates. Reaction monitoring by gel-phase 13C NMR using a 13C enriched BAL-linker // Tetrahedron Letters. 2002. Vol. 43. No. 19. pp. 3543-3546.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1016/S0040-4039(02)00564-6
UR - https://doi.org/10.1016/S0040-4039(02)00564-6
TI - Solid-phase syntheses of N-substituted carbamates. Reaction monitoring by gel-phase 13C NMR using a 13C enriched BAL-linker
T2 - Tetrahedron Letters
AU - Fernández-Forner, Dolors
AU - Huerta, Josep M
AU - Ferrer, Manel
AU - Casals, Gaspar
AU - Ryder, Hamish
AU - Giralt, E.
AU - Albericio, Fernando
PY - 2002
DA - 2002/05/01
PB - Elsevier
SP - 3543-3546
IS - 19
VL - 43
SN - 0040-4039
SN - 1873-3581
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2002_Fernández-Forner,
author = {Dolors Fernández-Forner and Josep M Huerta and Manel Ferrer and Gaspar Casals and Hamish Ryder and E. Giralt and Fernando Albericio},
title = {Solid-phase syntheses of N-substituted carbamates. Reaction monitoring by gel-phase 13C NMR using a 13C enriched BAL-linker},
journal = {Tetrahedron Letters},
year = {2002},
volume = {43},
publisher = {Elsevier},
month = {may},
url = {https://doi.org/10.1016/S0040-4039(02)00564-6},
number = {19},
pages = {3543--3546},
doi = {10.1016/S0040-4039(02)00564-6}
}
Cite this
MLA
Copy
Fernández-Forner, Dolors, et al. “Solid-phase syntheses of N-substituted carbamates. Reaction monitoring by gel-phase 13C NMR using a 13C enriched BAL-linker.” Tetrahedron Letters, vol. 43, no. 19, May. 2002, pp. 3543-3546. https://doi.org/10.1016/S0040-4039(02)00564-6.