Elsevier
Chemical Data Collections
,  volume 47 ,  pages 101064

Synthesis, crystal structure and Hirshfeld surface analysis of ethyl 4-hydroxy-2-(4-hydroxyphenyl)-1-methyl-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxylate

Fatin Nur Ain Abdul Rashid 1
, 
Siti Syaida Sirat 2, 3
, 
Husna Izzati Muhammad Nor Azharan 3
, 
Muhamad Zulfaqar Bacho 1
, 
Alexandra M. Z. Slawin 4
, 
Mohd Fazli Mohammat 1
, 
Mohd Fadhlizil Fasihi Mohd Aluwi 5
, 
Nor Saliyana Jumali 6
, 
Mohd Abdul Fatah Abdul Manan 7
1
 
2
 
3
 
4
 
5
 
6
 
7
 
Publication type: Journal Article
Publication date: 2023-10-01
Elsevier
scimago Q4
wos Q2
SJR: 0.116
CiteScore: 6.3
Impact factor: 2.7
ISSN: 24058300
General Chemistry
Abstract
Ethyl 4-hydroxy-2-(4-hydroxyphenyl)-1-methyl-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxylate, C14H15NO5(1) was synthesized via multicomponent reaction (MCR) of sodium diethyl oxalacetate, methylamine, and 4-hydroxybenzaldehyde. The structure of 1 was elucidated by using FT-IR, NMR and GCMS. These results were further confirmed by means of single crystal X-ray crystallography. The results showed that 1 was crystallized in orthorhombic space group Pca21 where a = 17.102(4), b = 9.923(2), c = 16.037(4), Å. The quantification of intermolecular interactions in the crystal structure was obtained by Hirshfeld surface analysis and showed that the H···H contacts were the most dominant interactions.
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Rashid F. N. A. A. et al. Synthesis, crystal structure and Hirshfeld surface analysis of ethyl 4-hydroxy-2-(4-hydroxyphenyl)-1-methyl-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxylate // Chemical Data Collections. 2023. Vol. 47. p. 101064.
GOST all authors (up to 50) Copy
Rashid F. N. A. A., Sirat S. S., Muhammad Nor Azharan H. I., Bacho M. Z., Slawin A. M. Z., Mohammat M. F., Mohd Aluwi M. F. F., Jumali N. S., Abdul Manan M. A. F. Synthesis, crystal structure and Hirshfeld surface analysis of ethyl 4-hydroxy-2-(4-hydroxyphenyl)-1-methyl-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxylate // Chemical Data Collections. 2023. Vol. 47. p. 101064.
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TY - JOUR
DO - 10.1016/j.cdc.2023.101064
UR - https://doi.org/10.1016/j.cdc.2023.101064
TI - Synthesis, crystal structure and Hirshfeld surface analysis of ethyl 4-hydroxy-2-(4-hydroxyphenyl)-1-methyl-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxylate
T2 - Chemical Data Collections
AU - Rashid, Fatin Nur Ain Abdul
AU - Sirat, Siti Syaida
AU - Muhammad Nor Azharan, Husna Izzati
AU - Bacho, Muhamad Zulfaqar
AU - Slawin, Alexandra M. Z.
AU - Mohammat, Mohd Fazli
AU - Mohd Aluwi, Mohd Fadhlizil Fasihi
AU - Jumali, Nor Saliyana
AU - Abdul Manan, Mohd Abdul Fatah
PY - 2023
DA - 2023/10/01
PB - Elsevier
SP - 101064
VL - 47
SN - 2405-8300
ER -
BibTex
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@article{2023_Rashid,
author = {Fatin Nur Ain Abdul Rashid and Siti Syaida Sirat and Husna Izzati Muhammad Nor Azharan and Muhamad Zulfaqar Bacho and Alexandra M. Z. Slawin and Mohd Fazli Mohammat and Mohd Fadhlizil Fasihi Mohd Aluwi and Nor Saliyana Jumali and Mohd Abdul Fatah Abdul Manan},
title = {Synthesis, crystal structure and Hirshfeld surface analysis of ethyl 4-hydroxy-2-(4-hydroxyphenyl)-1-methyl-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxylate},
journal = {Chemical Data Collections},
year = {2023},
volume = {47},
publisher = {Elsevier},
month = {oct},
url = {https://doi.org/10.1016/j.cdc.2023.101064},
pages = {101064},
doi = {10.1016/j.cdc.2023.101064}
}