Structure elucidation of a novel analogue of sildenafil detected as an adulterant in an herbal dietary supplement
Тип публикации: Journal Article
Дата публикации: 2007-04-01
scimago Q2
wos Q2
БС1
SJR: 0.628
CiteScore: 6.4
Impact factor: 3.1
ISSN: 07317085, 1873264X
PubMed ID:
17207601
Drug Discovery
Spectroscopy
Pharmaceutical Science
Clinical Biochemistry
Analytical Chemistry
Краткое описание
A new analogue of sildenafil was detected in an herbal dietary supplement, which was sold over the internet and promoted as a product for the enhancement of sexual performance. The structure of the compound was established using LC-MS, UV spectroscopy, MS-MS, and NMR. In addition, the compound was cleaved at its sulfonamide S-N bond yielding a sulfonic acid and an amine, which were independently characterized using LC-MS, GC-MS, and derivatization. The compound, named methisosildenafil, is a novel synthetic analogue of sildenafil in which the N-methylpiperazine moiety has been replaced with 2,6-dimethylpiperazine.
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Reepmeyer J. C., Woodruff J. B., d'Avignon D. Structure elucidation of a novel analogue of sildenafil detected as an adulterant in an herbal dietary supplement // Journal of Pharmaceutical and Biomedical Analysis. 2007. Vol. 43. No. 5. pp. 1615-1621.
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Reepmeyer J. C., Woodruff J. B., d'Avignon D. Structure elucidation of a novel analogue of sildenafil detected as an adulterant in an herbal dietary supplement // Journal of Pharmaceutical and Biomedical Analysis. 2007. Vol. 43. No. 5. pp. 1615-1621.
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TY - JOUR
DO - 10.1016/j.jpba.2006.11.037
UR - https://doi.org/10.1016/j.jpba.2006.11.037
TI - Structure elucidation of a novel analogue of sildenafil detected as an adulterant in an herbal dietary supplement
T2 - Journal of Pharmaceutical and Biomedical Analysis
AU - Reepmeyer, John C.
AU - Woodruff, Jeffrey B.
AU - d'Avignon, D André
PY - 2007
DA - 2007/04/01
PB - Elsevier
SP - 1615-1621
IS - 5
VL - 43
PMID - 17207601
SN - 0731-7085
SN - 1873-264X
ER -
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@article{2007_Reepmeyer,
author = {John C. Reepmeyer and Jeffrey B. Woodruff and D André d'Avignon},
title = {Structure elucidation of a novel analogue of sildenafil detected as an adulterant in an herbal dietary supplement},
journal = {Journal of Pharmaceutical and Biomedical Analysis},
year = {2007},
volume = {43},
publisher = {Elsevier},
month = {apr},
url = {https://doi.org/10.1016/j.jpba.2006.11.037},
number = {5},
pages = {1615--1621},
doi = {10.1016/j.jpba.2006.11.037}
}
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MLA
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Reepmeyer, John C., et al. “Structure elucidation of a novel analogue of sildenafil detected as an adulterant in an herbal dietary supplement.” Journal of Pharmaceutical and Biomedical Analysis, vol. 43, no. 5, Apr. 2007, pp. 1615-1621. https://doi.org/10.1016/j.jpba.2006.11.037.