, том 59 , издание 23 , страницы 2277-2280

Solvent-free mechanochemical Buchwald-Hartwig amination of aryl chlorides without inert gas protection

Qiao Ling Shao ¹

Zhi Jiang Jiang ¹

Weike Su ¹

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National Engineering Research Center for Process Development of Active Pharmaceutical Ingredients, Collaborative Innovation Center of Yangtze River Delta Region Green Pharmaceuticals, Zhejiang University of Technology, Hangzhou, 310014, PR China |

Тип публикации: Journal Article

Дата публикации: 2018-06-01

Elsevier

Tetrahedron Letters

scimago Q3

wos Q3

БС2

SJR: 0.334

CiteScore: 3.2

Impact factor: 1.5

ISSN: 00404039, 18733581

DOI: 10.1016/j.tetlet.2018.04.078

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Organic Chemistry

Drug Discovery

Biochemistry

Краткое описание

A solvent-free Buchwald-Hartwig amination had been developed under high-speed ball-milling conditions, which afforded the desired products with moderate to high yields. The addition of sodium sulfate was found to be crucial for improving both the performance and the reproducibility. Comparative solvent-free stirring experiments implicated the importance of mechanical interaction for the transformation, and the inert gas was proved to be unnecessary for this amination.

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Shao Q. L., Jiang Z. J., Su W. Solvent-free mechanochemical Buchwald-Hartwig amination of aryl chlorides without inert gas protection // Tetrahedron Letters. 2018. Vol. 59. No. 23. pp. 2277-2280.

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Shao Q. L., Jiang Z. J., Su W. Solvent-free mechanochemical Buchwald-Hartwig amination of aryl chlorides without inert gas protection // Tetrahedron Letters. 2018. Vol. 59. No. 23. pp. 2277-2280.

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TY - JOUR

DO - 10.1016/j.tetlet.2018.04.078

UR - https://doi.org/10.1016/j.tetlet.2018.04.078

TI - Solvent-free mechanochemical Buchwald-Hartwig amination of aryl chlorides without inert gas protection

T2 - Tetrahedron Letters

AU - Shao, Qiao Ling

AU - Jiang, Zhi Jiang

AU - Su, Weike

PY - 2018

DA - 2018/06/01

PB - Elsevier

SP - 2277-2280

IS - 23

VL - 59

SN - 0040-4039

SN - 1873-3581

ER -

BibTex |

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@article{2018_Shao,

author = {Qiao Ling Shao and Zhi Jiang Jiang and Weike Su},

title = {Solvent-free mechanochemical Buchwald-Hartwig amination of aryl chlorides without inert gas protection},

journal = {Tetrahedron Letters},

year = {2018},

volume = {59},

publisher = {Elsevier},

month = {jun},

url = {https://doi.org/10.1016/j.tetlet.2018.04.078},

number = {23},

pages = {2277--2280},

doi = {10.1016/j.tetlet.2018.04.078}

}

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Shao, Qiao Ling, et al. “Solvent-free mechanochemical Buchwald-Hartwig amination of aryl chlorides without inert gas protection.” Tetrahedron Letters, vol. 59, no. 23, Jun. 2018, pp. 2277-2280. https://doi.org/10.1016/j.tetlet.2018.04.078.

Издатель

Elsevier

Журнал

Tetrahedron Letters

scimago Q3

wos Q3

БС2

SJR

0.334

CiteScore

3.2

Impact factor

1.5

ISSN

00404039 (Print)

18733581 (Electronic)