Synthesis of 4-methoxy-3,5-dinitrobenzaldehyde: a correction to supposed tele nucleophilic aromatic substitution
Publication type: Journal Article
Publication date: 2003-05-01
scimago Q3
wos Q3
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
1,3-Dinitro-5-trichloromethylbenzene (2) was reacted with sodium methoxide in an attempt to prepare 4-methoxy-3,5-dinitrobenzaldehyde (7) via a reported tele nucleophilic aromatic substitution. The product from this reaction was methyl 3,5-dinitrobenzoate (5) and not the methoxy aldehyde as had been reported. The desired product was prepared by conventional nitration methodology from 4-methoxy-3-nitrobenzaldehyde.
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Monk K. A. et al. Synthesis of 4-methoxy-3,5-dinitrobenzaldehyde: a correction to supposed tele nucleophilic aromatic substitution // Tetrahedron Letters. 2003. Vol. 44. No. 19. pp. 3759-3761.
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Monk K. A., Siles R., Pinney K., Garner C. M. Synthesis of 4-methoxy-3,5-dinitrobenzaldehyde: a correction to supposed tele nucleophilic aromatic substitution // Tetrahedron Letters. 2003. Vol. 44. No. 19. pp. 3759-3761.
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RIS
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TY - JOUR
DO - 10.1016/s0040-4039(03)00751-2
UR - https://doi.org/10.1016/s0040-4039(03)00751-2
TI - Synthesis of 4-methoxy-3,5-dinitrobenzaldehyde: a correction to supposed tele nucleophilic aromatic substitution
T2 - Tetrahedron Letters
AU - Monk, Keith A.
AU - Siles, Rogelio
AU - Pinney, Kevin
AU - Garner, Charles M.
PY - 2003
DA - 2003/05/01
PB - Elsevier
SP - 3759-3761
IS - 19
VL - 44
SN - 0040-4039
SN - 1873-3581
ER -
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BibTex (up to 50 authors)
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@article{2003_Monk,
author = {Keith A. Monk and Rogelio Siles and Kevin Pinney and Charles M. Garner},
title = {Synthesis of 4-methoxy-3,5-dinitrobenzaldehyde: a correction to supposed tele nucleophilic aromatic substitution},
journal = {Tetrahedron Letters},
year = {2003},
volume = {44},
publisher = {Elsevier},
month = {may},
url = {https://doi.org/10.1016/s0040-4039(03)00751-2},
number = {19},
pages = {3759--3761},
doi = {10.1016/s0040-4039(03)00751-2}
}
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MLA
Copy
Monk, Keith A., et al. “Synthesis of 4-methoxy-3,5-dinitrobenzaldehyde: a correction to supposed tele nucleophilic aromatic substitution.” Tetrahedron Letters, vol. 44, no. 19, May. 2003, pp. 3759-3761. https://doi.org/10.1016/s0040-4039(03)00751-2.
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