Electrochemical synthesis and characterization of tantalum alkoxides
Тип публикации: Journal Article
Дата публикации: 2009-12-30
scimago Q1
wos Q1
БС1
SJR: 1.119
CiteScore: 8.1
Impact factor: 4.7
ISSN: 10036326, 22103384
Materials Chemistry
Metals and Alloys
Condensed Matter Physics
Geotechnical Engineering and Engineering Geology
Краткое описание
Tantalum(V) propoxide (Ta(OPr n ) 5 ), isopropoxide (Ta(OPr i ) 5 ) and butoxide(Ta(OBu n ) 5 ) were synthesized by electrochemical reactions of corresponding alcohol at sacrificial tantalum anode in the presence of tetraethylammonium chloride as a conductive additive. The pure products were isolated by reduced pressure distillation under 5 kPa. The crystal of Ta(OPr i ) 5 was obtained by recrystallization from hexane at −10 °C. These samples were characterized by Fourier transform infrared spectra (FT-IR), Raman spectra, nuclear magnetic resonance spectra (NMR), TG/DTA and ICP-MS. The results show that direct electrochemical synthesis of metal alkoxides has a high current efficiency and electrolysis yield. These alkoxides have a high purity of 99.97% and can be directly used as the precursor of Ta 2 O 5 films.
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Yang S. H. et al. Electrochemical synthesis and characterization of tantalum alkoxides // Transactions of Nonferrous Metals Society of China. 2009. Vol. 19. No. 6. pp. 1504-1508.
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Yang S. H., Cai Y., Yang H., Jin S. M. Electrochemical synthesis and characterization of tantalum alkoxides // Transactions of Nonferrous Metals Society of China. 2009. Vol. 19. No. 6. pp. 1504-1508.
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TY - JOUR
DO - 10.1016/s1003-6326(09)60060-1
UR - https://doi.org/10.1016/s1003-6326(09)60060-1
TI - Electrochemical synthesis and characterization of tantalum alkoxides
T2 - Transactions of Nonferrous Metals Society of China
AU - Yang, Sheng Hai
AU - Cai, Ya-Nan
AU - Yang, Hai-Ping
AU - Jin, Sheng Ming
PY - 2009
DA - 2009/12/30
PB - Elsevier
SP - 1504-1508
IS - 6
VL - 19
SN - 1003-6326
SN - 2210-3384
ER -
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@article{2009_Yang,
author = {Sheng Hai Yang and Ya-Nan Cai and Hai-Ping Yang and Sheng Ming Jin},
title = {Electrochemical synthesis and characterization of tantalum alkoxides},
journal = {Transactions of Nonferrous Metals Society of China},
year = {2009},
volume = {19},
publisher = {Elsevier},
month = {dec},
url = {https://doi.org/10.1016/s1003-6326(09)60060-1},
number = {6},
pages = {1504--1508},
doi = {10.1016/s1003-6326(09)60060-1}
}
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Yang, Sheng Hai, et al. “Electrochemical synthesis and characterization of tantalum alkoxides.” Transactions of Nonferrous Metals Society of China, vol. 19, no. 6, Dec. 2009, pp. 1504-1508. https://doi.org/10.1016/s1003-6326(09)60060-1.