Zr and Hf metallocenes. Study of the structure of a novel mononuclear zirconium trivalent organometallic
Publication type: Journal Article
Publication date: 1989-06-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Cp2∗MCl2, M Zr and Hf, were obtained by reaction of MCl4 with Cp∗Li, where Cp∗ 1,3-di-tertbutylcyclopentadienyl. Reduction of Cp2∗MCl2 with metallic potassium in pentane gave Cp2∗MCl. The molecular and crystal structure of Cp2∗ZrCl was established from X-ray diffraction; monoclinic, space group P21/b, a 12.722, b 16.336, c 13.426 A, γ 70.68°, R 0.065; monomeric Cp2∗ZrCl molecules, the average ZrC bond length is 2.505 A, that of ZrCl is 2.423 A, and the Cp∗centroidZrCp∗centroid angle is 133.3°.
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GOST
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Urazowski I. F. et al. Zr and Hf metallocenes. Study of the structure of a novel mononuclear zirconium trivalent organometallic // Journal of Organometallic Chemistry. 1989. Vol. 368. No. 3. pp. 287-294.
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Urazowski I. F., Ponomaryev V. I., Nifant'ev I. E., Lemenovskii D. A. Zr and Hf metallocenes. Study of the structure of a novel mononuclear zirconium trivalent organometallic // Journal of Organometallic Chemistry. 1989. Vol. 368. No. 3. pp. 287-294.
Cite this
RIS
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TY - JOUR
DO - 10.1016/0022-328X(89)85406-3
UR - https://linkinghub.elsevier.com/retrieve/pii/0022328X89854063
TI - Zr and Hf metallocenes. Study of the structure of a novel mononuclear zirconium trivalent organometallic
T2 - Journal of Organometallic Chemistry
AU - Urazowski, I F
AU - Ponomaryev, V I
AU - Nifant'ev, Ilya E.
AU - Lemenovskii, D A
PY - 1989
DA - 1989/06/01
PB - Elsevier
SP - 287-294
IS - 3
VL - 368
SN - 0022-328X
SN - 1872-8561
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{1989_Urazowski,
author = {I F Urazowski and V I Ponomaryev and Ilya E. Nifant'ev and D A Lemenovskii},
title = {Zr and Hf metallocenes. Study of the structure of a novel mononuclear zirconium trivalent organometallic},
journal = {Journal of Organometallic Chemistry},
year = {1989},
volume = {368},
publisher = {Elsevier},
month = {jun},
url = {https://linkinghub.elsevier.com/retrieve/pii/0022328X89854063},
number = {3},
pages = {287--294},
doi = {10.1016/0022-328X(89)85406-3}
}
Cite this
MLA
Copy
Urazowski, I. F., et al. “Zr and Hf metallocenes. Study of the structure of a novel mononuclear zirconium trivalent organometallic.” Journal of Organometallic Chemistry, vol. 368, no. 3, Jun. 1989, pp. 287-294. https://linkinghub.elsevier.com/retrieve/pii/0022328X89854063.