Defects and impurities in nanodiamonds: EPR, NMR and TEM study
A.M. Panich
1
,
W. Kempiński
2
,
A.E. Alexenskii
3
,
M. V. Baidakova
3
,
Vladimir Osipov
3
,
V.I. Siklitski
3
,
E. Osawa
4
,
M. Ozawa
4
,
1
2
3
Publication type: Journal Article
Publication date: 2002-11-01
scimago Q1
wos Q2
SJR: 0.816
CiteScore: 9.2
Impact factor: 4.9
ISSN: 00223697, 18792553
General Chemistry
Condensed Matter Physics
General Materials Science
Abstract
EPR, 13 C NMR and TEM study of ultradisperse diamond (UDD) samples is reported. The compounds show a high concentration of paramagnetic centers (up to 10 20 spin/g), which are due to structural defects (dangling C–C bonds) on the diamond cluster surface. The anomalous reduction in the spin–lattice relaxation time of 13 C (from several hours in natural diamond to ∼150 ms in UDD clusters) is attributed to the interaction between the unpaired electrons of the paramagnetic centers and nuclear spins. 13 C NMR line-width reflects the fact that the structure of the UDD surface is distorted in comparison to the ‘bulk’ diamond structure.
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Shames A. I. et al. Defects and impurities in nanodiamonds: EPR, NMR and TEM study // Journal of Physics and Chemistry of Solids. 2002. Vol. 63. No. 11. pp. 1993-2001.
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Shames A. I., Panich A., Kempiński W., Alexenskii A., Baidakova M. V., Dideikin A. T., Osipov V., Siklitski V., Osawa E., Ozawa M., Vul' A. Defects and impurities in nanodiamonds: EPR, NMR and TEM study // Journal of Physics and Chemistry of Solids. 2002. Vol. 63. No. 11. pp. 1993-2001.
Cite this
RIS
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TY - JOUR
DO - 10.1016/S0022-3697(02)00185-3
UR - https://linkinghub.elsevier.com/retrieve/pii/S0022369702001853
TI - Defects and impurities in nanodiamonds: EPR, NMR and TEM study
T2 - Journal of Physics and Chemistry of Solids
AU - Shames, Alexander I.
AU - Panich, A.M.
AU - Kempiński, W.
AU - Alexenskii, A.E.
AU - Baidakova, M. V.
AU - Dideikin, Artur Torievich
AU - Osipov, Vladimir
AU - Siklitski, V.I.
AU - Osawa, E.
AU - Ozawa, M.
AU - Vul', A.Ya.
PY - 2002
DA - 2002/11/01
PB - Elsevier
SP - 1993-2001
IS - 11
VL - 63
SN - 0022-3697
SN - 1879-2553
ER -
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BibTex (up to 50 authors)
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@article{2002_Shames,
author = {Alexander I. Shames and A.M. Panich and W. Kempiński and A.E. Alexenskii and M. V. Baidakova and Artur Torievich Dideikin and Vladimir Osipov and V.I. Siklitski and E. Osawa and M. Ozawa and A.Ya. Vul'},
title = {Defects and impurities in nanodiamonds: EPR, NMR and TEM study},
journal = {Journal of Physics and Chemistry of Solids},
year = {2002},
volume = {63},
publisher = {Elsevier},
month = {nov},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0022369702001853},
number = {11},
pages = {1993--2001},
doi = {10.1016/S0022-3697(02)00185-3}
}
Cite this
MLA
Copy
Shames, Alexander I., et al. “Defects and impurities in nanodiamonds: EPR, NMR and TEM study.” Journal of Physics and Chemistry of Solids, vol. 63, no. 11, Nov. 2002, pp. 1993-2001. https://linkinghub.elsevier.com/retrieve/pii/S0022369702001853.