Methylene acetals as protecting groups — an improved preparation method
Publication type: Journal Article
Publication date: 1997-06-01
scimago Q3
wos Q3
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
A facile method to protect vic diols, 1,3 diols and other hydroxyl functions as methylene acetals is achieved by treating the relative substrates with POCl3 or SOCl2 in DMSO. The good yields obtained, the good solubility of many organic compounds in DMSO and the easy hydrolysis of the 1,3,5-trioxaepane derivatives prepared from trans vic diols make useful this protecting method.
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Total citations:
23
Citations from 2025:
1
(4.35%)
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MLA
Cite this
GOST
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Guiso M. et al. Methylene acetals as protecting groups — an improved preparation method // Tetrahedron Letters. 1997. Vol. 38. No. 24. pp. 4291-4294.
GOST all authors (up to 50)
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Guiso M., Procaccio C., Fizzano M. R., Piccioni F. Methylene acetals as protecting groups — an improved preparation method // Tetrahedron Letters. 1997. Vol. 38. No. 24. pp. 4291-4294.
Cite this
RIS
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TY - JOUR
DO - 10.1016/S0040-4039(97)00882-4
UR - https://doi.org/10.1016/S0040-4039(97)00882-4
TI - Methylene acetals as protecting groups — an improved preparation method
T2 - Tetrahedron Letters
AU - Guiso, Marcella
AU - Procaccio, Carmela
AU - Fizzano, Maria Rosaria
AU - Piccioni, Francesco
PY - 1997
DA - 1997/06/01
PB - Elsevier
SP - 4291-4294
IS - 24
VL - 38
SN - 0040-4039
SN - 1873-3581
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{1997_Guiso,
author = {Marcella Guiso and Carmela Procaccio and Maria Rosaria Fizzano and Francesco Piccioni},
title = {Methylene acetals as protecting groups — an improved preparation method},
journal = {Tetrahedron Letters},
year = {1997},
volume = {38},
publisher = {Elsevier},
month = {jun},
url = {https://doi.org/10.1016/S0040-4039(97)00882-4},
number = {24},
pages = {4291--4294},
doi = {10.1016/S0040-4039(97)00882-4}
}
Cite this
MLA
Copy
Guiso, Marcella, et al. “Methylene acetals as protecting groups — an improved preparation method.” Tetrahedron Letters, vol. 38, no. 24, Jun. 1997, pp. 4291-4294. https://doi.org/10.1016/S0040-4039(97)00882-4.